Hydrous fluids play a vital role in the chemical and rheological evolution of ductile, quartz-bearing continental crust, where fluid percolation pathways are controlled by grain boundary domains. In this study, widths of grain boundary domains in seven quartzite samples metamorphosed under varying crustal conditions were investigated using Atomic Force Microscopy (AFM) which allows comparatively easy, high magnification imaging and precise width measurements. It is observed that dynamic recrystallization at higher metamorphic grades is much more efficient at reducing grain boundary widths than at lower temperature conditions. The concept of force-distance spectroscopy, applied to geological samples for the first time, allows qualitative estimation of variations in the strength of grain boundary domains. The strength of grain boundary domains is inferred to be higher in the high grade quartzites, which is supported by Kernel Average Misorientation (KAM) studies using Electron Backscatter Diffraction (EBSD). The results of the study show that quartzites deformed and metamorphosed at higher grades have narrower channels without pores and an abundance of periodically arranged bridges oriented at right angles to the length of the boundary. We conclude that grain boundary domains in quartz-rich rocks are more resistant to fluid percolation in the granulite rather than the greenschist facies.

The Remal granite gneiss body in the southeastern part of the Singhbhum Craton, near its contact with the Rengali Province, preserves two orthogonal penetrative foliations. The subhorizontal foliation defines cross and trough bedding structures, and is characterized by (i) systematic grain-size variation between the layers, (ii) the presence of feldspar laths and (iii) graphic intergrowth textures, confirming that it is primary and of igneous origin (Sign). Sign has a non-planar geometry and shows a spread in orientations, while a later foliation of tectonic origin is defined by alternating biotite-rich and biotite poor bands that define a consistently oriented gneissic foliation (S1). S1 gneissic layering is associated with the alignment of biotite flakes and myrmekite formation, and operated under low grade metamorphic conditions. S1 shows a remarkable similarity in orientation with the shear fabric along the amalgamation front of the Rengali Province with the Eastern Ghats Province further to the south, indicating that strain related to this regional strike-slip event can be identified even in southeastern Singhbhum.

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