Recebido em 23/8/07; aceito em 3/7/08; publicado na web em 24/10/08 CHEMICAL CONSTITUENTS ISOLATED FROM THE WOOD OF Senna reticulata Willd. (LEGUMINOSEAE). The phytochemical investigation of the wood extracts of Senna reticulata (Leguminoseae) yielded six anthraquinones: chrysophanol, physcion, aloe-emodin, 1,3,8-trihydroxyanthraquinone, 3-methoxy-1,6,8-trihydroxyanthraquinone, emodin and the chrysophanol-10,10' bianthrone. The triterpenes α and β-amirin, the steroids β-sitosterol and stigmasterol as well as the flavonoid kaempferol were also identified. The structures were established by spectral analysis, including two-dimensional NMR techniques. It is the first report of 1,3,8-trihydroxyanthraquinone and 3-methoxy-1,6,8-trihydroxyanthraquinone in higher plants.

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Os intensos períodos de estiagem e pela concentração que a água adquire quando os níveis dos reservatórios estão baixos torna-se evidente a ausência da qualidade da água consumida pela população. O estudo teve como objetivo avaliar os parâmetros físico-químicos e microbiológicos da água para consumo no município de Itapiúna-CE. Estudo do tipo experimental, prospectivo, transversal e com abordagem do tipo qualitativo e quantitativo. Foram analisadas 4 amostras de 500 mL cada, uma do Açude Castro e de três locais escolhidos nas residências de pontos estratégicos de distribuição pela concepcionária, da água usada para consumo no município de Itapiúna-CE no mês de outubro de 2016. Para seleção das amostras foram adotados os critérios de inclusão: água do açude castro (Amostra A), e três amostras de residências, consideradas a água retirada diretamente do registro da Cagece, escolhidas aleatoriamente dos bairros do município. As amostras apresentaram cloretos alterados quando comparadas às quantidades estabelecidas pela Portaria 2914/2011 do Ministério da Saúde (MS). A respeito aos parâmetros como Sólidos Totais, Condutividade, Cloreto e Dureza, os valores também encontrou-se valores superiores. A amostra A (Açude Castro) obteve pH de 8.81 e apresentou alcalinidade devido a carbonatos (80 mgCO3/L) e a bicarbonatos (150mg CaCO3/L). Verificou-se que 50% das amostras apresentaram presença de coliformes totais e coliformes fecais, evidenciando contaminação da maioria das amostras analisadas. Contudo, de acordo com as análises realizadas, as amostras não obedecem ao padrão de potabilidade, tornando á água imprópria para o consumo humano. PHYSICAL-CHEMICAL AND MICROBIOLOGICAL QUALITY OF WATER FOR CONSUMPTION IN RESIDENCES OF A TOWN IN THE SERTÃO CENTRAL ABSTRACT Factors such as long periods of drought and the physical and chemical characteristics of water influence in the quality of water consumed by the population, leading to health problems. This study aimed at evaluating the physical-chemical and microbiological parameters of water for consumption in the town of Itapiúna-CE. Four samples of 500 mL each were analyzed, one from Açude Castro and three from chosen places in the residences of strategic sites of distribution by the water company for consumption in the town of Itapiúna-CE in October 2016. For sample selection it was adopted the inclusion criteria: water from Açude Castro (sample A), and three samples of residences, considered the water withdrawn directly from Cagece register, randomly chosen from neighborhoods of the town. The samples present altered chlorides compared to the established quantities by the Consolidation Ordinance No. 5 of September 28, 2017 of the Ministry of Health (MS). Regarding the parameters such as total solids, conductivity, chloride and hardness, were also found higher values. Sample A (Açude Castro) obtained pH of 8.81 and presented alkalinity due to carbonates (80 mgCO3 / L) and bicarbonates (150 mg CaCO3 / L). It was verified that 50% of the samples presented total coliforms and fecal coliforms, evidencing contamination of most of the samples analyzed. So, according to the analysis carried out, the samples did not obey the standard of potable water, making the water unfit for human consumption.

Objective: to evaluate the efficiency of water treatment filters using activated carbon from different sources of biomass residue. Methods: this is a descriptive experimental study of a quantitative nature carried out at the Centro Universitário Católica de Quixadá, Ceará-Brazil, during the period from January to June 2018. Activated carbon filters were prepared, and subsequently, their efficiency in water treatment was evaluated. Wood waste, green coconut husk, cashew nut shell, and bamboo stem were used as a source of raw material. The water treatment filter was assembled using the column chromatography method by adding sand and cotton as other filter media. Physicochemical parameters were used to evaluate the efficiency of the built filters. Results: principal component analysis selected two water quality components, explaining 80.081% of the total variance. The cophenetic correlation coefficient of r=0.9572 indicates that the estimated dendrogram was good, considering the water quality parameters. Among the filters, bamboo showed the best response among the filters tested, being responsible for the reduction of several factors such as color, turbidity, total hardness, and sodium. Conclusion: activated carbon filters derived from discarded wood and cashew nut shells had little influence on improving water quality compared to the control sample