An effective heterojunction
with robust charge separation and enormous
degradation efficiency is the major task for photocatalyst preparation.
In this study, we have prepared the FeCo
2
O
4
-loaded
g-C
3
N
4
nanosheet by the sol–gel-assisted
calcination method for photo-Fenton-like degradation under visible-light
irradiation by activating persulfate. The nanocomposite exhibits a
higher charge separation efficiency than pure g-C
3
N
4
and FeCo
2
O
4
for the degradation reaction
against naproxen drugs. An effective interaction between the nanoparticles
increases the degradation efficiency up to 91% with a synergistic
index of 73.62%. Moreover, the nanocomposite exhibits a 78% mineralization
efficiency against the naproxen pollutant under visible-light irradiation.
For practical implementation, the degradation reaction was tested
with various pH values, different water sources (DI, lake, and tap
water), and light sources (LED (visible)/direct sunlight (UV–visible)).
Moreover, the possible degradation mechanism predicted by the elemental
trapping experiment and the recycling experiment clearly revealed
that the heterojunction composite has a high enough degradation stability.
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