The precipitation of the y', y" and 6 phases in a spray-formed version of IN 7 18 has been studied by hardness measurement and metallographic examination of samples subjected to solution treatment at 1025°C followed by isothermal treatments between 620 and 1010°C up to 100 h. The precipitation processes were compared to those in a wrought (ring-rolled) version of the alloy subjected to the same heat treatments. Time-temperature-hardness diagrams for the two alloys were constructed. Small differences were observed between the two materials but these can at least partly be attributed to differences in composition. For the spray-cast material the &phase solvus temperature was determined and the growth kinetics of the y" phase established Suprralloys 71 8. 625.
In the weld repair cycles of alloy 718 the solution temperature is usually selected low enough to avoid grain growth in wrought material. At such low temperatures, however, δ-phase also precipitates and the amount increases with each repair cycle.It is well understood that the overall ductility is reduced by the presence of the δ-phase in alloy 718 and, as such, may reduce the weldability. But it is also reported that the δ-phase may cause incipient melting in grain boundaries at the heat affected zone, HAZ, through a niobium rich melt fed by the local abundance of this element from attached δ−platelets. The purpose of the present work is to shed light on this issue on the one hand through practical weld experiments under heavily constrained circumstances and on the other through high temperature ductility testing in special hot tensile test equipment by which the hot ductility of re-melted material also was possible to examine. Materials with two levels of δ-phase and with two grain sizes were included.Contrary to what was anticipated it was extremely difficult to provoke cracking even in inhomogeneous cast material at the highest δ−levels in heavily constrained TIG-weld experiments. Also the hot ductility test results, measured as the high temperature ductility recovery temperature and range, indicated that there is no or very limited deterioration by the presence of δ-phase. Anomalous results, however, much lower ductility recovery temperatures, were found in samples with large grain size and a small amount of δ-phase. For re-melted samples several hundred degrees lower recovery temperatures were measured.
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