PURPOSE The aims of this study were to investigate mechanical properties and hydrothermal degradation behaviour of the cubic-containing translucent yttrium oxide stabilized tetragonal zirconia polycrystal (Y-TZP). MATERIALS AND METHODS Four groups of Y-TZP (T, ST, XT, and P), containing different amount of cubic crystal, were examined. Specimens were aged by autoclaving at 122℃ under 2 bar pressure for 8 h. Phase transformation was analyzed using X-ray diffraction (XRD) to measure phase transformation (t→m). Kruskal-Wallis test was used to determine the difference. Surface hardness, biaxial flexural strength, and fracture toughness in values among the experimental groups and verified with Wilcoxon matched pairs test for hardness values and Mann Whitney U for flexural strength and fracture toughness. RESULTS XRD analysis showed no monoclinic phase in XT and P after aging. Only Group T showed statistically significant decreases in hardness after aging. Hydrothermal aging showed a significant decrease in flexural strength and fracture toughness in group T and ST, while group XT and P showed no effect of aging on fractural strength and fracture toughness with P <.05. CONCLUSION Hydrothermal aging caused reduction in mechanical properties such as surface hardness, biaxial flexural strength, and fracture toughness of Y-TZP zirconia. However, cubic-containing zirconia (more than 30% by volume of cubic crystal) was assumed to have high resistance to hydrothermal degradation. Clinical significance: Cubic-containing zirconia could withstand the intraoral aging condition. It could be suggested to use as a material for fabrication of esthetic dental restoration.
Zirconia, a crystalline oxide of zirconium, holds good mechanical, optical, and biological properties. The metal-free restorations, mostly consisting of all-ceramic/zirconia restorations, are becoming popular restorative materials in restorative and prosthetic dentistry choices for aesthetic and biological reasons. Dental zirconia has increased over the past years producing wide varieties of zirconia for prosthetic restorations in dentistry. At present, literature is lacking on the recent zirconia biomaterials in dentistry. Currently, no article has the latest information on the various zirconia biomaterials in dentistry. Hence, the aim of this article is to present an overview of recent dental zirconia biomaterials and tends to classify the recent zirconia biomaterials in dentistry. This article is useful for dentists, dental technicians, prosthodontists, academicians, and researchers in the field of dental zirconia.
Objective This study investigated the effect of hydrothermal aging on surface roughness and translucency of various translucent zirconia materials. Materials and Methods Four types of zirconia were tested. Group 1 was translucent zirconia with no cubic structure. Group 2, 3, and 4 included cubic-containing zirconia with different amounts of cubic structures (less than 30%, 30–50%, and more than 50%, respectively). Each group contained 15 disk-shape specimens with dimensions of 15 mm in diameter and 1 mm in thickness. As-sintered surface roughness, translucency parameter, and contrast ratio were evaluated in the two different sessions, before and after aging. Statistical Analysis Two-way repeated measures ANOVA with Bonferroni test was used to analyze statistically significant difference in those tested parameters. Phase structure before and after aging was analyzed by X-ray diffraction analysis (XRD). Results Groups 1 and 2 showed significant increased surface roughness after aging while groups 3 and 4 showed no alteration of surface. There was no effect of aging on translucency in all groups. After aging, group 1 and 2 presented monoclinic structure (16.63 and 5.01%, respectively). Conclusion Hydrothermal aging caused phase transformation and increasing surface roughness in group 1 and 2 but did not affect translucency in all groups.
Objective The aim of this study is to investigate the fatigue and hydrothermal degradation behavior among the cubic-containing translucent yttrium oxide stabilized tetragonal zirconia polycrystal (Y-TZP). Materials and Methods Four groups of commercial Y-TZP (T, ST, XT, and P), containing different amount of cubic crystal, were examined. Artificial aging was accomplished by autoclaving at 122°C under 2 bar pressure for 8 hours. Fatigue simulation parameters were set using an axial 50 N load, a total of 240,000 cycles. Flexural fatigue strength was evaluated.Statistical analysis: Two-way analysis of variance with Tukey's honestly significant difference test was used to determine the difference in fatigue strength values between various type of zirconia materials within control and aging with a significant level of 5%. Weibull analysis was conducted on the fatigue strength data. Results All groups showed the mean flexural fatigue strength had no significant difference in hydrothermally aged specimens compared with specimens without aging (p = 0.154). Group T showed significantly higher flexural fatigue strength followed by group ST, XT, and P. Group XT and P showed no significant difference in strength value (p > 0.05). Group T demonstrated a lower probability of failure than group ST, XT, and P whether with or without aging. Weibull modulus in group T and ST with aging condition was increased and higher than all the experimental groups. Conclusion Cubic-containing zirconia materials (group ST, XT, and P) exhibited lower flexural fatigue strength than non-cubic 3Y-TZP zirconia (group T). However, various cubic-containing translucent zirconia was assumed to have high resistance to hydrothermal degradation.
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