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In this study, high energy synchrotron radiation was used to perform an in-situ diffraction experiment in medium Mn Fe-6Mn-0.5C-1Al alloy to study the elemental partitioning and consequent austenite phase evolution at different stages, namely, during heating, holding and cooling. It has been observed that the austenite phase fraction significantly increases on annealing at the inter-critical annealing temperature and remains stable at room temperature. The austenite phase stability at room temperature is due to the rapid partitioning of manganese (Mn) and carbon (C) during annealing. The relative change in d-spacing (Δd/d) during heating-cooling confirms the partitioning of alloying elements during inter-critical annealing.

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By applying cold extrusion, an elemental metal powder composite Al60Mg40 was prepared. The texture gradient was measured over the cross-section of the extrusion profile using synchrotron radiation while the bulk texture was obtained by neutron diffraction. The aluminum phase shows a typical texture component of plane-strain deformation in the middle part of the sample and a uniaxial deformation texture at the surface. In the central region of the extruded bar, the (0002) Mg pole figure shows a split along the extrusion direction (±ED), which also has been observed in rare-earth containing magnesium alloys. These two poles twist towards the transverse direction on moving towards the surface of the extruded bar; one pole moves to +TD and the other one to −TD. The angle of twist increases towards the TD surface.