In order to improve the tensile properties of additively manufactured Ti 6Al 4V parts, specific heat treatments have been developed. Previous work demonstrated that a sub-transus thermal treatment at 920°C followed by water quenching generates a dual-phase α+α′ microstructure with a high work-hardening capacity inducing a desirable increase in both strength and ductility. The present study investigates the micromechanical behavior of this α+α′ material as well as the thermal stability of the metastable α' martensite. To that end, annealing of the α+α′ microstructure is performed and the resulting microstructural evolution is analyzed, along with its impact on the tensile properties. A deeper understanding of the micromechanics of the multiphase microstructure both before and after annealing is achieved by performing in-situ tensile testing within a SEM, together with digital image correlation for full-field local strain measurements. This approach allows the strain partitioning to be quantified at a microscale and highlights a significant mechanical contrast between the two phases. In the α+α′ microstructure, the α′ phase is softer than the α phase, which is confirmed by nanoindentation measurements. Partial decomposition of the martensite during annealing induces a substantial hardening of the α′ phase, which is attributed to fine-scale precipitation and solution strengthening. A scale transition model based on the iso-work assumption and describing the macroscopic tensile behavior of the material depending on the individual mechanical behavior of each phase is also proposed. This model enables to provide insights into the underlying deformation and work-hardening mechanisms.
To improve the mechanical properties of additively manufactured parts, specific heat treatments must be developed. Annealing of electron beam-melted Ti-6Al-4V was performed at sub-transus temperatures and followed by water quenching. Such treatments generate an α + α dual-phase microstructure. Microstructural and mechanical characterizations revealed that the heat-treated specimens show a broad range of tensile properties, depending on the fraction of martensite. The specimens treated between 850°C and 920°C exhibit an increase in strength and ductility, which is related to a remarkable hardening behavior. Work-hardening is attributed to kinematic hardening arising from the mechanical contrast between the α and α phases.
IMPACT STATEMENTInnovative heat treatments leading to α + α dual-phase microstructures are developed on Ti-6Al-4V parts produced by additive manufacturing. They lead to unprecedented work-hardening capabilities for this alloy.
Thermoelectric materials are ranked by their ability to meet a criterion of excellence that is related to their conversion efficiency. This dimensionless figure of merit, zT = (σS 2 T)/κ, measures how well a
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