Metal additive manufacturing (AM) is on its way to industrialization. One of the most promising techniques within this field, electron beam melting (EBM), is nowadays used mostly for the fabrication of high-performance Ti-based alloy components for the aerospace and medical industry. Among the industrial applications envisioned for the future of EBM, the fabrication of high carbon steels for the tooling industry is of great interest. In this context, the process windows for dense and crack-free specimens for a highly alloyed (Cr-Mo-V) coldwork steel powder are presented in this article. High-solidification rates during EBM processing lead to very fine and homogeneous microstructures. The influence of process parameters on the resulting microstructure and the chemical composition is investigated. In addition, preliminary results show very promising mechanical properties regarding the as-built and heat-treated microstructure of the obtained material.
Electron beam melting (EBM) is currently hampered by the low number of materials available for processing. This work presents an experimental study of process parameter development related to EBM processing of stainless steel alloy 316LN. Area energy (AE) input and beam deflection rate were varied to produce a wide array of samples in order to determine which combination of process parameters produced dense (>99%) material. Both microstructure and tensile properties were studied. The aim was to determine a process window which results in dense material. The range of AE which produced dense materials was found to be wider for 316LN than for many other reported materials, especially at lower beam deflection rates. Tensile and microstructural analysis showed that increasing the beam deflection rate, and consequently lowering the AE, resulted in material with a smaller grain size, lower ductility, lower yield strength, and a narrower window for producing material that is neither porous nor swelling.
This work focuses on the possibility of processing stainless steel 316LN powder into lightweight structures using electron beam melting and investigates mechanical and microstructural properties in the material of processed components. Lattice structures conforming to ISO13314:2011 were manufactured using varying process parameters. Microstructure was examined using a scanning electron microscope. Compression testing was used to understand the effect of process parameters on the lattice mechanical properties, and nanoindentation was used to determine the material hardness. Lattices manufactured from 316L using EBM show smooth compression characteristics without collapsing layers and shear planes. The material has uniform hardness in strut shear planes, a microstructure resembling that of solid 316LN material but with significantly finer grain size, although slightly coarser sub-grain size. Grains appear to be growing along the lattice struts (e.g., along the heat transfer direction) and not in the build direction. Energydispersive x-ray spectroscopy analysis reveals boundary precipitates with increased levels of chromium, molybdenum and silicon. Studies clearly show that the 316LN grains in the material microstructure are elongated along the dominating heat transfer paths, which may or may not coincide with the build direction. Lattices made from a relatively ductile material, like 316LN, are much less susceptible to catastrophic collapse and show an extended range of elastic and plastic deformation. Tests indicate that EBM process for 316LN is stable allowing for both solid and lightweight (lattice) structures.
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