We report the results of the characterization of Cu oxide thin films deposited by radio frequency (r.f.) magnetron sputtering at different annealing temperatures. The deposited Cu oxide thin films were investigated by scanning electron microscopy, spectroscopic ellipsometry, X-ray diffraction, atomic force microscopy, Xray photoelectron spectroscopy, and contact angle measurements. The thickness of the films was about 180 nm and the monoclinic CuO phase was detected. The CuO 2 and Cu(OH) 2 phases were grown as amorphous phase and the ratio of the three phases were independent on the annealing temperature. The surface of Cu oxide films changed from hydrophilic to hydrophobic as the annealing temperature increased. This phenomenon is due to the increase of the surface roughness. The direct optical band gap was also obtained and laid in the range between 2.36 and 3.06 eV.
Dual pulse rocket motor has a rocket motor with different pulse grains divided by a pulse separation device such as a fragile bulkhead or a thermal barrier type. It distributes thrust energy very effectively via pulse separation device to improve range and terminal velocity of a missile. This paper contains the thermal barrier design and experimental analysis through ground firing tests of small dual pulse motors. The results will be applied to the design, test and evaluation of the scale up dual pulse rocket motor.
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