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-This work presents aspects of the parastillation process, which employs a unique distillation column where the vapor stream is divided into two equal parts and the falling liquid is alternately in contact with both vapor parts on a stage-by-stage basis. A laboratory-scale apparatus was used to study the parastillation column. Experiments were carried out under total and partial reflux conditions using an ethanolwater system. Experiments were conducted to analyze the effects of vapor flow rate and initial ethanol concentration in the reboiler on the hydrodynamic conditions. Limiting operating conditions were defined. Murphree separation efficiencies were calculated and discussed.

-The purpose of this work was to study the mass transfer performance of rotating packed beds applying the "Higee" process. The operations were carried out with the n-hexane/n-heptane distilling system at atmospheric pressure and under total reflux conditions. The rotating speed could be varied between 300 and 2500 rpm, which provided centrifugal forces from 5 to 316 times the Earth's gravity. The effects of concentration, vapor velocity, rotating speed and packing type (two different Raschig ring sizes and structured wire mesh packing) on mass transfer behavior were analyzed. Experimental results showed that the mass transfer coefficient depends on the liquid flow rates and rotating speed. The equipment had high separation efficiency in a reduced bed volume.

This paper investigates some aspects of the parastillation process, which employs a unique distillation column. A laboratory scale apparatus was used to study the parastillation column. Experiments were carried out under total and partial reflux conditions, using an ethanol‐water system. Experiments were conducted to analyze the influence of the vapour flow rate and reboiler initial ethanol concentration on the hydrodynamic conditions. Limiting operating conditions were defined. Murphree separation efficiencies were calculated and discussed.