Oxide dispersion strengthened (ODS) ferritic steels typically contain a fine dispersion of nanoscopic Y(Al, Ti) oxides, leading to an improvement in mechanical and physical properties. A rapid prototyping technique, selective laser melting (SLM), was successfully applied to consolidate as-mechanically alloyed ODS-PM2000 (Fe-19Cr-5.5Al-0.5Ti-0.5Y 2 O 3 ; all wt.%) powder to fabricate solid and thin-walled builds of different thickness. This work is intended to act as a first study to investigate the tensile response of such configurations at room temperature, using miniaturized test specimens along and perpendicular to the growth direction. The 0.2% offset yield strength of as-grown wall builds was inferior to conventional PM2000 alloy (recrystallized), but could be significantly increased by conducting post-build heat treatments. Young's modulus and yield strength showed anisotropy and were enhanced when testing perpendicular to the build growth direction. Electron backscatter diffraction revealed a strong [0 0 1] fibre texture along the growth direction, which explains the anisotropic behaviour. Additionally, studies on the morphology of the individual fracture surfaces, the grain structure of the cross-section near this region and the size distribution of ODS particles in such builds were conducted. A fine dispersion of precipitates was retained in all SLM builds, and findings suggest that a certain amount of Y is probably still in atomic solution in the as-grown condition and forms new small nanoscopic dispersoids during annealing, which lead to enhanced strengthening.
Oxide dispersion strengthened (ODS) alloys exhibit superior mechanical and physical properties due to the presence of nanoscopic Y(Al, Ti) oxide precipitates, but their manufacturing process is complex. The present study is aimed at further investigation of the application of an alternative, Additive Manufacturing (AM) technique, Selective Laser Melting (SLM), to the production of consolidated ODS alloy components. Mechanically alloyed PM2000 (ODS-FeCrAl) powders have been consolidated and a fine dispersion of Y-containing precipitates were observed in an as built thinwalled component, but these particles were typically poly-crystalline and contained a variety of elements including O, Al, Ti, Cr and Fe. Application of post-build heat treatments resulted in the modification of particle structures and compositions; in the annealed condition most precipitates were transformed to single crystal yttrium aluminium oxides. During the annealing treatment, precipitate distributions homogenised and localised variations in number density were diminished. The resulting volume fractions of those precipitates were 25-40% lower than have been reported in conventionally processed PM2000, which was attributed to Y-rich slag-like surface features and inclusions formed during SLM.
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