A detailed study on vertical electropolishing (VEP) of a 1.3-GHz single-cell niobium coupon cavity, which contains six coupons and four viewports at different positions, is reported. The cavity was vertically electropolished using a conventional rod and three types of unique cathodes named as Ninja cathodes, which were designed to have four retractable blades made of either an insulator or a metal or a combination of both. This study reveals the effect of the cathodes and their rotation speed on uniformity in removal thickness and surface morphology at different positions inside the cavity. Removal thickness was measured at several positions of the cavity using an ultrasonic thickness gauge and the surface features of the coupons were examined by an optical microscope and a surface profiler. The Ninja cathode with partial metallic blades was found to be effective not only in reducing asymmetric removal, which is one of the major problems in VEP and might be caused by the accumulation of hydrogen (H 2) gas bubbles on the top iris of the cavity, but also in yielding a smooth surface of the entire cavity. A higher rotation speed of the Ninja cathode prevents bubble accumulation on the upper iris, and might result in a viscous layer of similar thickness in the cavity cell. Moreover, a higher electric field at the equator owing to the proximity of partial metallic blades to the equator surface resulted in a smooth surface. The effects of H 2 gas bubbles and stirring were also observed in lab EP experiments.
The authors report a detail study on the emission properties of field emitter array (FEA) of micro-circular emitters of multiwall carbon nanotubes (CNTs). The FEAs were fabricated on patterned substrates prepared with an array of circular titanium (Ti) islands on titanium nitride coated tantalum substrates. CNTs were rooted into these Ti islands to prepare an array of circular emitters. The circular emitters were prepared in different diameters and pitches in order to optimize their structure for acquiring a high emission current. The pitch was varied from 0 to 600 μm, while a diameter of circular emitters was kept constant to be 50 μm in order to optimize a pitch. For diameter optimization, a diameter was changed from 50 to 200 μm while keeping a constant edge-to-edge distance of 150 μm between the circular emitters. The FEA with a diameter of 50 μm and a pitch of 120 μm was found to be the best to achieve an emission current of 47 mA corresponding to an effective current density of 30.5 A/cm2 at 7 V/μm. The excellent emission current was attributed to good quality of CNT rooting into the substrate and optimized FEA structure, which provided a high electric field on a whole circular emitter of 50 μm and the best combination of the strong edge effect and CNT coverage. The experimental results were confirmed with computer simulation.
Electropolishing (EP) is a standard process for the treatment of the interior surface of niobium (Nb) superconducting radio-frequency (SRF) cavities used in particle accelerators. We previously conducted a study on vertical electropolishing (VEP), in which the cavity was set vertically during EP of a 1.3 GHz Nb single-cell cavity. In that study, we showed that the major cause of asymmetric removal in VEP is the accumulation of hydrogen gas bubbles, generated during the EP process, on the upper half cell of the cavity. Three types of unique rotating cathodes were tested with the aim to resolve the issues of asymmetric removal and rough surface. Appropriate cathode design and parameters reduced the asymmetric removal in the cell and yielded a smooth surface of the cavity. In this study, we have performed an extensive investigation on VEP of both single-and nine-cell Nb 1.3 GHz cavities with a modified cathode. The VEP parameters with single-and nine-cell coupon cavities were investigated, which facilitate an in situ study of the coupon currents at various positions of the cavities and observation from the viewports located near the iris and equator positions of the cavities. The modified cathode and optimized VEP process for the singlecell cavity yielded uniform removal in the cavity cell and a smooth surface of the interior of the cavity. A novel acid flow method that allows the separation of the acid flow in the cavity and cathode housing was employed in the nine-cell cavity to efficiently remove the gas bubbles from the cavity. The optimized acid flow rates in the cavity and cathode housing, along with other adequate parameters including temperature, cathode rotation speed, and applied voltage, made the surface smooth and significantly reduced the removal nonuniformity in the nine-cell cavity. The single-and nine-cell cavities after an average removal of 46 and 130 μm, respectively, were tested in a vertical cryostat. The single-and nine-cell cavities achieved 31 MV=m at a Q 0 value of 9 × 10 9 and 28.3 MV=m at a Q 0 value of 6.7 × 10 9 , respectively, in the rf tests at the temperature of 2 K. The achieved SRF performances were as good as the baseline performances achieved after the horizontal electropolishing process of the same cavities.
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