In this paper we report a new sol–gel method for the fabrication of
MgB2 films.
Polycrystalline MgB2
films were prepared by spin-coating a precursor solution of
Mg(BH4)2 diethyl
ether on (001)Al2O3
substrates followed with annealing in Mg vapor. In comparison with the
MgB2 films grown
by other techniques, our films show medium qualities including a superconducting transition temperature of
TC ∼ 37 K, a critical current
density of JC(5 K, 0 T) ∼ 5 × 106 A cm − 2, and
a critical field of HC2(0) ∼ 19 T. Such a sol–gel technique shows potential in the commercial fabrication of practically used
MgB2 films as
well as MgB2
wires and tapes.
5A02 aluminium alloy was joined by transient liquid phase (TLP) bonding using the two-step heating process as follows: the faying area was first heated to 600uC and kept for 5 s and then cooled down to 595uC and kept for 3 min. The microstructure and properties of the joint were investigated and compared with that of conventional TLP bond at 595uC for 3 min. The results show that the two-step heating process can produce a wave bond line that is different from the planar interface associated with conventional TLP bonding at a constant temperature. The defects at the bond line are greatly reduced, and metal to metal contacts are established along the wave bond line using the two-step heating process. Therefore, the tensile strength and bending ductility of the joint are dramatically improved.
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