Because of the limitation of mining techniques and economic conditions, large amounts of residual coal resources have been left in underground coal mines around the world. Currently, with mining technology gradually developing, residual coal can possibly be remined. However, when residual coal is remined, caving areas might form, which can seriously affect the safety of coal mining. Hence, grouting technology is put forward as one of the most effective technologies to solve this problem. To study the grouting diffusion in fractured rock mass, this paper developed a visualization platform of grouting diffusion and a three-dimensional grouting experimental system that can monitor the grout diffusion range, diffusion time and grout pressure; then, a grouting experiment is conducted based on this system. After that, the pattern of the grouting pressure variation, grout flow and grout diffusion surface are analyzed. The relationship among some factors, such as the grouting diffusion radius, compressive strength of the grouted gravel, porosity, water-cement ratio, grouting pressure, grouting time, permeability coefficient and level of grout, is quantitatively analyzed by using MATLAB. The study results show that the flow pattern of the grout in fractured porous rock mass has a parabolic shape from the grouting hole to the bottom. The lower the level is, the larger the diffusion range of the grout is. The grouting pressure has the greatest influence on the grouting diffusion radius, followed by the grouting horizon and water-cement ratio. The grouting permeability coefficient has the least influence on the grouting diffusion radius. The grout water-cement ratio has the greatest influence on the strength of the grouted gravel, followed by the grouting permeability. The grouting pressure coefficient has the least amount of influence on the grouting diffusion radius. According to the results, the grouting parameters are designed, and a layered progressive grouting method is proposed. Finally, borehole observation and a core mechanical property test are conducted to verify the application effect. This grouting technology can contribute to the redevelopment and efficient utilization of wasted underground coal resources.

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The shear behavior of rock discontinuities controls the stability of rock masses to a great extent. In this paper, laboratory shear tests were performed on rock-like materials with different cracks to study the effect of nonpersistent joints on the shear behavior of rock masses. The results show that the variation trends of the shear stress-displacement curves of specimens with different cracks are generally similar and have the same stage characteristics. When the crack length is relatively short, the elastic stage is prolonged, the peak shear strength decreases, and the shear displacement corresponding to the peak shear strength and the residual shear strength increases with the increase of the crack length. When the crack length is relatively long, the elastic stage is shortened, the peak shear strength decreases, and the shear displacement corresponding to the peak shear strength increases with the increase of the crack length. The peak shear stress gradually decreases with the increase of the crack length. The shear strength of the specimens with unilateral cracks is much higher than that of the specimens with bilateral cracks. The shear strength of the specimens is affected not only by the crack length but also by the crack distribution. The acoustic emission (AE) count peak occurs when the shear stress drops sharply and has an inverse “S”-type variation trend with the increase of the crack length. The inclination angle of the fracture decreases, the roughness of the fracture surface decreases, and the proportion of the wear area on the fracture surface increases gradually with the increase of the crack length. The AE source decreases with the increase of the crack length, and their locations are obviously asymmetric. This work can greatly contribute to the insight into the shear failure mechanism of rock discontinuities with nonpersistent joints.

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Thermodynamic hydrate inhibitors (THIs) are often used in marine gas field operations to prevent the formation of natural gas hydrate (NGH), and it is important to study the effect of THIs on hydrate synthesis characteristics. Herein, the effects of water (H2O), sodium chloride (NaCl), and ethylene glycol (EG) on NGH synthesis characteristics under different initial pressure conditions are tested using the self‐developed 1D NGH production simulation test system. The effects of each THI on the maximum synthesis rate and maximum synthesis amount of NGH are investigated using two physical quantities, peak of temperature increment and maximum gas conversion rate. The results show that the 2.65 wt% salt solution has the minimum inhibition effect on the maximum synthesis rate of NGH, and the solution with a 3:1 mixture of H2O and EG has the maximal inhibition effect on the maximum synthesis rate of NGH. When only H2O and EG or H2O and NaCl are present in the reactor, the higher the concentration of EG or NaCl, the more significant is the inhibition effect on the maximum synthesis amount of NGH.