No abstract

Fe3O4 nanoparticles were prepared by coprecipitation method. Microwave synthesis method changed the property of the surface of chitosan, and the carboxymethyl chitosan was prepared. The carboxymethyl chitosan magnetic nanoparticle was prepared by microwave synthesis. Carboxymethyl chitosan magnetic nanoparticles were characterized by IR and SEM methods. The application conditions are discussed. Using this material to separate the alkaloid of Evodia rutaecarpa will greatly shorten the time than traditional separation method. The components will be more pure.

Alumina is the most promising ceramic armor material and SHPB testing is typically used to investigate dynamic deformation behaviour and ballistic mechanisms. In this research the effect of the incident wave shaping technique on the stress equilibrium state during testing was analysed. The compressive strength of alumina ceramic materials was evaluated under high strain rate compressive loads of 1200-1800/s. The SHPB compression strength was found to increase with decreasing grain size to a maximum of 3.80±0.25 GPa, and the ceramic materials studied exhibited high strain-rate sensitive mechanical properties due to crack tip inertia effects.

The silica gel surface was alkylated by silane coupling agent KH-570 under the microwave assisted and orthogonal experiment was adopted to optimize the silica gel surface silanized experimental conditions with synthetic yield as index. With quercetin as the template molecule, 4 - vinyl pyridine as the functional monomer, ethylene glycol dimethyl acrylate as the cross linking agent, azodiisobutyronitrile as initiator, under the microwave assisted in silane silicone surface quercetin molecularly imprinted polymer was successfully synthesized. Take selected quercetin as index, another orthogonal experiment was implemented to optimize the quercetin-selective MIPs synthesis experiment on silica gel surface. What is more, the adsorptive property of quercetin-selective MIPs which was grafted on silica gel surface has been inspected. We have extracted of quercetin in the ethyl acetate from raspberry with quercetin-selective MIPs grafted on silica gel surface. Synthetic time have been shortened more than a dozen times, the efficiency of preparation of MIPs have been greatly improved.

No abstract