Epoxy resin and polyetheretherketone (PEEK) resin were decomposed into their monomers such as phenol, cresols, and their analogues by thermal treatment in sub-and supercritical water in a 10-ml tubing bomb reactor. The addition of basic compounds such as Na 2 CO 3 was effective in promoting the decomposition reaction of the resins. In the reaction of epoxy resin, the yield of identified products reached 10% for the reaction at 703 K over 1 h. In the reaction of PEEK resin, the total yield of phenol and dibenzofuran reached 88% for the reaction at 703 K over 3 h. Chemical participation of water in the decomposition reaction was confirmed by the reaction of dinaphthylether.
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