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Bangladesh is a densely populated agricultural country. A wide range of products of pesticides being used in Bangladesh is already considered a health and environmental concern by different international agencies including the World Health Organization (WHO). Excessive, irrational use of pesticides in agriculture, and lack of knowledge on pest management have caused widespread pesticide pollution which is now posing a substantial threat to the environment and local people. In this review, we assessed and analyzed previous literature systematically to map a complete scenario of pesticide pollution in Bangladesh, covering soil, water, and foods. Most of the previous studies indicated that soil, water, and different seasonal vegetables are contaminated with organophosphorus, pyrethroid, and exceeded the FAO/WHO maximum residual limits. Concentration of chlorpyriphos, malathion were found below the detection limit in soil samples. But water samples were found contaminated with chlorpyrifos, diazinon, malathion, carbaryl and carbofuran. Considered vegetable samples were adulterated with fenvalerate, quinalphos, cypermethrin, fenitrothion, dimethoate, parathion, linuron, phenthoate. Persistence of organochlorines in the environment is limited and meets the maximum residue level (MRLs). This study will help to depict the pesticide pollution status in the environmental matrices in recent years and to cut off the exacerbation of pesticide pollution. A proactive approach is essential to limit the pesticide pollution load in the environmental matrices.

Ionic liquid-based hollow-fiber liquid–liquid–liquid microextraction (IL-HF-LLLME) coupled to capillary electrophoresis (CE) has been developed for the determination of six sulfonamides (SAs) in aquaculture waters. A series of extraction parameters was optimized to enhance the extraction efficiency, which included type and pore size of hollow fiber, type and composition of extraction solvent, pH value of donor phase, the concentration of acceptor phase and the mass ratio of donor phase to acceptor phase along with extraction temperature and time. Under optimal conditions, the IL-HF-LLLME-CE method provided a wide liner range for six SAs from 2 to 1,000 μg L−1 (r2 ≥ 0.9995), the limits of the detection from 0.25 to 0.48 and the enrichment factors from 122 to 230, respectively. Relative standard deviations for intra- and interday precision were 1.4–5.3% and 1.8–7.5% (n = 5), respectively. The proposed method was successfully applied for the determination of trace-level SAs in seven real-world aquaculture water samples with good recoveries (80.4–100.7%). Also, sulfamerazine and sulfamethoxazole were detected at the level of 0.52–1.60 μg L−1 in two water samples. Due to its good sensitivity, simple operation, short analysis time and eco-friendliness, the developed method has a great application potential in analysis of trace SA residues in aquaculture waters.

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