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Volatiles of milk were characterized by solid-phase microextraction coupled with comprehensive twodimensional gas chromatography and time-of-flight mass spectrometry. Comprehensive two-dimensional gas chromatography with time-of-flight mass spectrometry two-dimensional gas chromatography with time-of-flight mass spectrometry not only separated the 52 compounds that co-elute in conventional gas chromatography-mass spectrometry, but also identified 107 compounds that were first reported in milk. These volatiles included aliphatic hydrocarbons (69), aromatic hydrocarbons (42), ketones (28), esters (16), aldehydes (14), alcohols (14), acids (14), nitrogenous compounds (9), ethers (8), and sulfo compounds (3). Five dominant volatiles were hexanoic acid (193.57 ng/mL milk), methoxy-phenyl-oxime (114.83 ng/mL milk), octanoic acid (109.38 ng/mL milk), 4,5-dimethyl-1hexene (101.48 ng/mL milk), and 2-Pentanone (99.74 ng/mL milk). This proposes an improvement methodology for determining the volatiles of dairy products.

The quantitative relationships among chemical composition, storage temperature, and texture of cheese were not fully understood. In this study, the effects of composition and temperature on textural properties of eight common varieties of sliced cheese were examined. The textural properties of sliced cheeses, including firmness, cohesiveness, adhesiveness, springiness, chewiness, and resilience, were measured by texture profile analysis after storage at 4 and 25°C for 4 h. Multivariate logistic regression models were established to describe the quantitative relationships of textural properties (dependent variables) to chemical composition and storage temperature (independent variables) of sliced cheeses. Results showed that protein, fat, moisture, and sodium chloride contents as well as storage temperature significantly affected the texture of sliced cheeses (P<0.05). In particular, fat in the dry matter and moisture in the nonfat substances were negatively correlated with firmness of sliced cheeses (P<0.05). As storage temperature rose from 4 to 25°C, the average values of firmness, chewiness, and resilience substantially declined by 42%, 45%, and 17%, respectively (P<0.05). This study provided reference data for adjusting chemical composition and storage temperature of common cheese products to obtain favorable texture for Chinese consumers, which thereby facilitated the localization of cheese industry in Chinese market.

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