Slim titanate naotubes was prepared from industrial coarse TiO2 powder by simple sonochemical-hydrothermal processing. The influences of ultrasonic irradiation on TiO2 precursors were investigated. The morphology and crystal structure of the products were characterized by TEM and X-ray diffraction, respectively. The typical products are long nanotubes around 8-10nm in out diameter. Both anatase and rutile TiO2 precursors can be transferred into titanate nanotubes in this sonochemical & hydrothermal processing.
A novel process, gel-tape-casting, is employed to fabricate LSGM thin dense sheets in aqueous AM system. The influences of powder properties, dispersant and other additives were discussed and relevant processing parameters were also explored. The slurry of LSGM with a high solid loading about
33 vol.% was successfully obtained.
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