In this work we represent the results for the development of proton conductive membranes by radiochemical modification of thin PVDF films with their subsequent sulfonation. Radiation source were 4He ions with energy of 27 MeV produced by cyclotron R-7M the FTI TPU. The results of IR-spectroscopy, gravimetric analysis and microscopy are represented to evaluate changes in membranes properties. It was shown that the deepness of modificated gel can be controlled by radiation.
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