The set of composite materials that consist of micro/nanocellulose and complex K2Eu(MoO4)(PO4) luminescent oxide particles was prepared. The composites were studied by means of scanning electron microscopy, XRD analysis, dilatometry, differential scanning calorimetry and thermogravimetric analysis, and dielectric and luminescence spectroscopy.Dependencies of density, crystallinity, relative extension, thermal extension coefficient, dielectric relaxation parameters, intensity and shape of photoluminescence bands on temperature, and content of oxide component were studied. The structure of the composite without oxide is formed by grains of nearly 5–50 μm in size (crystallinity is about ~56%). Structure of the micro/nanocellulose samples which contain oxide particles is similar, but the cellulose grains are deformed by oxide particles. Dependencies of the abovementioned properties on temperature and oxide content were analyzed together with data on the size distribution of oxide particles for the samples for various oxide and molecules of water concentrations.
Morphology and photoluminescence (PL) properties for microcrystalline cellulose (MCC), microcrystalline nitrite powders of common formulae MNO 2 (M = Na, K) (MCN) and two-component materials composed of both MCC and MCN have been prepared and characterized by means of optical microscopy and luminescence spectroscopy. This study aimed to clarify a possibility of low-limit determination of the nitrite traces in water solutions by luminescent method.Published by Copernicus Publications on behalf of the AMA Association for Sensor Technology.
Surface morphology and photoluminescence (PL) properties of both microcrystalline cellulose (MCC), microcrystalline powders of the alkali metals nitrites MNO2 (M = Na. K, Cs) (MCN) and two-component composite materials based on the MCC and MCN have been studied and characterized by means of optical microscopy and luminescence spectroscopy.
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