3D-printed dissolvable inserts for efficient and customizable fabrication of NMR transceiver coils

Kelz, Jessica I.; Kelly, John; Martin, Rachel W.

doi:10.1016/j.jmr.2019.06.008

Cited by 26 publications

(9 citation statements)

References 19 publications

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“…Specifically, we extend high throughput screening to include granular solids. This work adds to the reports demonstrating the usefulness of 3D printing in organic chemistry, including assembly of custom NMR coils, microreactors, and flow-cell spectrometers …”

Section: Discussionmentioning

confidence: 87%

3D-Printed Labware for High-Throughput Immobilization of Enzymes

et al. 2020

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In continuous flow biocatalysis, chemical transformations can occur under milder, greener, more scalable, and safer conditions than conventional organic synthesis. However, the method typically involves extensive screening to optimize each enzyme's immobilization on its solid support material. The task of weighing solids for large numbers of experiments poses a bottleneck for screening enzyme immobilization conditions. For example, screening conditions often require multiple replicates exploring different support chemistries, buffer compositions, and temperatures. Thus, we report 3D-printed labware designed to measure and handle solids in multichannel format and expedite screening of enzyme immobilization conditions. To demonstrate the generality of these advances, alkaline phosphatase, glucose dehydrogenase, and laccase were screened for immobilization efficiency on seven resins. The results illustrate the requirements for optimization of each enzyme's loading and resin choice for optimal catalytic performance. Here, 3D-printed labware can decrease the requirements for an experimentalist's time by >95%. The approach to rapid optimization of enzyme immobilization is applicable to any enzyme and many solid support resins. Furthermore, the reported devices deliver precise and accurate aliquots of essentially any granular solid material.

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Section: Discussionmentioning

confidence: 87%

3D-Printed Labware for High-Throughput Immobilization of Enzymes

et al. 2020

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“…[ 13,14 ] 3D printing and NMR do not end here: you can print sample tubes for solid‐state NMR, [ 15 ] whole NMR magnets, [ 16 ] and even scaffolds for making NMR coils. [ 17–19 ] A review on 3D printing in NMR can be found here. [ 20 ]…”

Section: Phase One: Printingmentioning

confidence: 99%

“…[13] solid-state NMR, [15] whole NMR magnets, [16] and even scaffolds for making NMR coils. [17][18][19] A review on 3D printing in NMR can be found here. [20] Fixing broken plastic laboratory objects has also become extremely easy, and many pipette holders or pipette parts, connectors, and desk organizers are freely downloadable from repositories.…”

Section: Phase One: Printingmentioning

confidence: 99%

A 3D Printer in the Lab: Not Only a Toy

Saggiomo

2022

Advanced Science

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Although 3D printers are becoming more common in households, they are still under‐represented in many laboratories worldwide and regarded as toys rather than as laboratory equipment. This short review wants to change this conservative point of view. This mini‐review focuses on fused deposition modeling printers and what happens after acquiring your first 3D printer. In short, these printers melt plastic filament and deposit it layer by layer to create the final object. They are getting cheaper and easier to use, and nowadays it is not difficult to find good 3D printers for less than €500. At such a price, a 3D printer is one, if not the most, versatile piece of equipment you can have in a laboratory.

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“…[13,14] 3D printing and NMR do not end here: you can print sample tubes for solid-state NMR, [15] whole NMR magnets, [16] and even scaffolds for making NMR coils. [17][18][19] A review on 3D printing in NMR can be found here [20]. Fixing broken plastic laboratory objects has also become extremely easy, and many pipette holders or pipette parts, connectors, and desk organizers are freely Saggiomo | ChemRχiv | May 5, 2022 | 1-10 Fig.…”

Section: Phase 1: Printingmentioning

confidence: 99%

A 3D Printer in the lab: not only a toy

Saggiomo

2022

Preprint

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Although 3D printers are becoming more common in households, they are still underrepresented in many laboratories worldwide and regarded as toys rather than as laboratory equipment. This short review wants to change this conservative point of view. This mini-review focuses on Fused Deposition Modeling (FDM) printers and what happens after acquiring your first 3D printer. In short, these printers melt plastic filament and deposit it layer by layer to create the final object. They are getting cheaper and easier to use, and nowadays it is not difficult to find good 3D printers for less than 500€. At such a price, a 3D printer is one, if not the most, versatile piece of equipment you can have in a laboratory.

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3D-printed dissolvable inserts for efficient and customizable fabrication of NMR transceiver coils

Cited by 26 publications

References 19 publications

3D-Printed Labware for High-Throughput Immobilization of Enzymes

3D-Printed Labware for High-Throughput Immobilization of Enzymes

A 3D Printer in the Lab: Not Only a Toy

A 3D Printer in the lab: not only a toy

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