1995
DOI: 10.1080/10575639508043206
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A New Flavonol Glycoside from Eucalyptus globulous Subsp. Maidenii

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Cited by 6 publications
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“…Acid hydrolysis afforded rhamnose as the sugar residue. Its 1 H NMR data showed a 2H AX and a 3H ABX system characteristic of quercetin moiety [11] while the UV data recorded in MeOH and with addition of common shift reagents [8,9] suggested that the residual sugar was attached at C-3 position of the aglycone, a fact further supported by HMBC correlations as outlined in Acid hydrolysis. Compounds (1-4), 15 mg each in a mixture of 8% HCl (2 mL) and MeOH (20 mL) were separately refluxed for 2 h. The reaction mixtures were reduced under pressure to dryness, dissolved in H 2 O (3 mL) and neutralized with NaOH.…”
Section: Resultsmentioning
confidence: 84%
“…Acid hydrolysis afforded rhamnose as the sugar residue. Its 1 H NMR data showed a 2H AX and a 3H ABX system characteristic of quercetin moiety [11] while the UV data recorded in MeOH and with addition of common shift reagents [8,9] suggested that the residual sugar was attached at C-3 position of the aglycone, a fact further supported by HMBC correlations as outlined in Acid hydrolysis. Compounds (1-4), 15 mg each in a mixture of 8% HCl (2 mL) and MeOH (20 mL) were separately refluxed for 2 h. The reaction mixtures were reduced under pressure to dryness, dissolved in H 2 O (3 mL) and neutralized with NaOH.…”
Section: Resultsmentioning
confidence: 84%