2017
DOI: 10.1016/j.scitotenv.2017.07.039
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Analysis of emerging organic contaminants in water, fish and suspended particulate matter (SPM) in the Joint Danube Survey using solid-phase extraction followed by UHPLC-MS-MS and GC–MS analysis

Abstract: Highlights71 water samples from the Danube River and its tributaries were analysed.Most relevant micropollutants were benzotriazoles, pharmaceuticals, organophosphorus compounds, and PFOS/A.PFOS concentrations exceed its environmental quality standard (EQS).Concentrations and loads are similar for the years 2007 and 2013.

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Cited by 108 publications
(42 citation statements)
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“…Perfluoroalkyl and polyfluoroalkyl substances (PFASs) are highly fluorinated chemicals used in a variety of applications and consumer products (Robel et al 2017;Tokranov et al 2018), which can result in their emission to the environment (Wang et al 2017). Due to concerns on environmental and health impacts of PFASs, monitoring surveys have assessed the extent of contamination of aquatic ecosystems (Lindim et al, 2015;Campo et al, 2016;Loos et al, 2017) and water sources (Hu et al, 2016;Boone et al, 2019). Certain PFASs such as perfluorooctane sulfonate (PFOS) are found at widespread scale, including in the open ocean and polar regions (Yeung et al, 2017;Rigét et al, 2019).…”
Section: Introductionmentioning
confidence: 99%
“…Perfluoroalkyl and polyfluoroalkyl substances (PFASs) are highly fluorinated chemicals used in a variety of applications and consumer products (Robel et al 2017;Tokranov et al 2018), which can result in their emission to the environment (Wang et al 2017). Due to concerns on environmental and health impacts of PFASs, monitoring surveys have assessed the extent of contamination of aquatic ecosystems (Lindim et al, 2015;Campo et al, 2016;Loos et al, 2017) and water sources (Hu et al, 2016;Boone et al, 2019). Certain PFASs such as perfluorooctane sulfonate (PFOS) are found at widespread scale, including in the open ocean and polar regions (Yeung et al, 2017;Rigét et al, 2019).…”
Section: Introductionmentioning
confidence: 99%
“…Therefore, solid samples require preliminary treatment, i.e., decomposition. The advantage of the liquid sample is primarily its homogeneity and the possibility of dosing smaller amounts during the analysis [34,35].…”
Section: Current Stage In Research Problemsmentioning
confidence: 99%
“…In the majority of cases, separation has been performed on various C columns [ 4 , 10 , 11 , 21 , 37 , 38 , 39 ], although columns with phenyl stationary phase have also been used [ 2 , 8 , 22 ]. Usually, the mobile phase has initially a high water content and is then gradually adjusted to raise the ratio of organic solvent, this solvent being either methanol (MeOH) [ 10 , 40 ], acetonitrile (ACN) [ 22 , 32 ] or both [ 38 , 41 ]. The critical problem of the LC is the separation of 4- and 5-methyl-benzotriazole isomers, due to their similar retention.…”
Section: Analytical Techniques For the Determination Of Polar Benzmentioning
confidence: 99%