Organic Syntheses 2003
DOI: 10.1002/0471264180.os052.03
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Azoethane

Abstract: Azoethane intermediate: N,N ′‐ Diethylsulfamide product: Azoethane solvent: petroleum ether intermediate: N,N ′‐dicyclohexylsulfamide … Show more

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Cited by 6 publications
(10 citation statements)
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“…The additives are readily obtained from the basic bleach oxidation of the corresponding sulfamides as described in Scheme 1. [14] The higher-molecular-weight dicyclohexyl diazenyl derivative 2 is prepared to minimize the risk of volatilization during extrusion of poly(propylene).…”
Section: Resultsmentioning
confidence: 99%
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“…The additives are readily obtained from the basic bleach oxidation of the corresponding sulfamides as described in Scheme 1. [14] The higher-molecular-weight dicyclohexyl diazenyl derivative 2 is prepared to minimize the risk of volatilization during extrusion of poly(propylene).…”
Section: Resultsmentioning
confidence: 99%
“…Compounds 1 0 and 1 were prepared according to a slightly modified procedure described in the literature. [14] Synthesis of N,N 0 -Bis(cyclohexyl)sulfamide 1 0 Under a nitrogen atmosphere, a solution of sulfuryl chloride (10.0 mL, 121 mmol) in 40 mL of dichloromethane was added dropwise at 0 8C to a solution of cyclohexylamine (30.0 g, 303 mmol) and triethylamine (84.0 mL, 606 mmol) in 150 mL of dichloromethane. Upon completion of the addition, the reaction mixture was stirred for 4 h at 0 8C.…”
Section: General Considerationsmentioning
confidence: 99%
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“…However, most Lissotriton fossils have been reported without description or depiction (e.g. B€ ohme, 2003;B€ ohme & Ilg, 2003) precluding an assessment of their reliability. The first well-documented finds of Lissotriton include L. aff.…”
Section: Divergence Datingmentioning
confidence: 99%
“…While the economic impacts of a college or university are varied and far-reaching, they can be considered as either effects on knowledge creation, research and development, or as effects of the direct and indirect expenditures flowing into the surrounding economy (Stokes & Coomes, 1998). Institutional studies have been conducted to illuminate the former impact and thus describe the economic effects of the transmission and discovery of knowledge and ideas, conducting pure and applied research, and the development of new technologies and industries (Ohme, 2003). While these studies estimate the effect on the labor market in both the short-term and long-term, other studies investigate the latter effects of economic impact created by the institution's pur-chasing of goods and services from within its local economy (Parsons & Griffiths, 2003).…”
Section: Literature Reviewmentioning
confidence: 99%