Characterisation of coloured TiO /Ti/glass systems

Skowroński, Łukasz; Trzciński, Marek; Antończak, Arkadiusz J.; Domanowski, P.; Kustra, M.K.; Wachowiak, W.; Naparty, M.K.; Hiller, Tomasz; Bukaluk, A.; Wronkowska, A. A.

doi:10.1016/j.apsusc.2014.10.050

Cited by 24 publications

(9 citation statements)

References 27 publications

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“…Its thickness was established to be 2 nm. The optical constants of glass substrate were established in the separate experiment [12,13].…”

Section: Xrd Measurementsmentioning

confidence: 99%

“…This means that the kinetic energy of gas phase particles is practically not dissipated before their condensation on the substrate. The GIMS method was successfully used to produce decorative multilayers [12][13][14][15][16]. The recent investigation clearly shows that applying the GIMS technique allows for synthesizing the nanocrystalline rutile phase of TiO 2 directly during the deposition on the unheated substrate [17].…”

Section: Introductionmentioning

confidence: 99%

“…It should be noted that microstructural properties of Ti coatings prepared under different conditions and using various modifications of magnetron sputtering methods are described in literature [2][3][4][5][6][7][18][19][20][21]; however, their optical constants and/or opto-electronic properties are described only in a few publications [20,[22][23][24]. Additionally, the results related to the optical constants of Ti can b found in Reference [12,14,15]. It should be noted that the optical properties (the complex dielectric function, reflectance and transmittance spectra) of semitransparent titanium coatings (the thickness of a layer below 50 nm) were described in Reference [13,14].…”

Section: Introductionmentioning

confidence: 99%

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Optical Properties of Titanium in the Regime of the Limited Light Penetration

Skowroński

2020

Materials

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In this study, the titanium layers from 12 to 1470 nm thick were fabricated by using the method involving dynamically changed working gas pressure (gas injection magnetron sputtering). The influence of the deposition time on the optical and electrical properties of Ti films, as well as on their microstructure, are considered. The samples are investigated by means of spectroscopic ellipsometry, atomic force microscopy, X-ray diffraction, and confocal optical microscopy. Additionally, for the Ti layers, the sheet resistance was determined. The produced coatings exhibit privileged direction of growth (002). The obtained results show a gradual increase in the mean relaxation time of free-carriers with the increase in the thickness of titanium film. However, the plasma energy exhibits maximum for the coating with the thickness of 93 nm. For such thickness, the lowest value of optical resistivity (about 200 μ Ω cm) was observed. It was found that the dc- and optical resistivity exhibit similar values for titanium films with thickness up to 93 nm. For thicker Ti layers, significant differences in resistivities (dc- and optical) were noticed. The behavior of the Drude parameter (the plasma energy), calculated optical resistivity, and discrepancies between values of optical and dc-resistivities for thicker Ti coatings can be explained as a result of the limited light penetration.

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“…Its thickness was established to be 2 nm. The optical constants of glass substrate were established in the separate experiment [12,13].…”

Section: Xrd Measurementsmentioning

confidence: 99%

Section: Introductionmentioning

confidence: 99%

Section: Introductionmentioning

confidence: 99%

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Optical Properties of Titanium in the Regime of the Limited Light Penetration

Skowroński

2020

Materials

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“…Dalam teknologi yang memerlukan pemeriksaan secara visual, kod warna merupakan kaedah yang dapat memberikan maklumat dengan cepat serta warna merupakan kaedah yang paling mudah dalam menyampaikan struktur dan bentuk bahan. Warna telah digunakan secara meluas dalam industri kaca dan seramik (Boschetti et al 2016;Holgado et al 2016;Jovaní et al 2016;Kim & Kim 2016;Mantovani et al 2015;Möncke et al 2014;Nor et al 2016;Skowroński et al 2014;Thieme et al 2016). Terdapat kajian yang cuba untuk mewarnakan sambungan pempaterian (King & Gulino 1998;Zeng et al 2011) untuk pelbagai aplikasi (Jiang et al 2007;Kim 2000;Kim & Cho 1995).…”

Section: Pengenalanunclassified

Kesan Pigmen Pewarna terhadap Pertumbuhan Sebatian antara Logam Sambungan Pateri Sn-3.0Ag-0.5Cu

Jalar¹,

Bakar

Ismail

et al. 2018

JSM

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Pewarnaan pes pateri membuka suatu ruang kepada keperluan dalam teknologi untuk proses pengenalpastian, penandaan, piawaian, pengujian dan penilaian terhadap antarasambungan pes pateri. Dua jenis pigmen pewarna iaitu hijau (G) dan bercahaya dalam gelap (GD) digunakan untuk mengkaji kesan pewarnaan sambungan pateri ke atas kestabilan antarasambungan pateri Sn-3.0Ag-0.5Cu (SAC 305). Pes pateri tanpa warna digunakan sebagai sampel kawalan untuk membandingkan keputusan kajian. Uji kaji penuaan sesuhu digunakan untuk melihat perubahan pertumbuhan sebatian antara logam (IMC). Pigmen pewarna GD dengan peratusan sebanyak 5% telah menunjukkan kestabilan pertumbuhan IMC dengan perubahan pertumbuhan yang paling rendah iaitu sebanyak 5.6 µm bagi sambungan pateri yang berwarna berbanding dengan peratusan pigmen pewarna yang lebih tinggi dengan perubahan pertumbuhan IMC sehingga 9 µm selepas didedahkan kepada penuaan sesuhu pada 150°C selama 1000 jam. Walau bagaimanapun, kestabilan pertumbuhan IMC dengan penggunaan pes pateri berwarna adalah lebih rendah berbanding dengan pes pateri tidak berwarna. Maka penambahan pigmen pewarna hendaklah dipertimbangkan dengan mengambil kira kestabilan mikrostruktur dan pertumbuhan lapisan IMC supaya tidak menjejaskan kualiti dan kebolehharapan sesuatu sambungan pateri.

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“…al. [22] have proposed an interesting variant of producing colored coatings deposited by the GIMS technology on glass substrates by the use of two thin layers Ti/TiO 2 colored coatings. In the system, the 300 nm thick Ti layers played a role of a reflective undercoat while the color of the coating was the result of the light interference taking place in the area of transparent TiO 2 layer deposited on the Ti undercoat.…”

Section: Introductionmentioning

confidence: 99%

Novel GIMS technique for deposition of colored Ti/TiO₂ coatings on industrial scale

Zdunek

Skowroński

Choduń

et al. 2016

Materials Science-Poland

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The aim of the present paper has been to verify the effectiveness and usefulness of a novel deposition process named GIMS (Gas Injection Magnetron Sputtering) used for the first time for deposition of Ti/TiO 2 coatings on large area glass substrates covered in the condition of industrial scale production. The Ti/TiO 2 coatings were deposited in an industrial system utilizing a set of linear magnetrons with the length of 2400 mm each for covering the 2000 × 3000 mm glasses. Taking into account the specific course of the GIMS (multipoint gas injection along the magnetron length) and the scale of the industrial facility, the optical coating uniformity was the most important goal to check. The experiments on Ti/TiO 2 coatings deposited by the use of GIMS were conducted on substrates in the form of glass plates located at the key points along the magnetrons and intentionally non-heated during any stage of the process. Measurements of the coatings properties showed that the thickness and optical uniformity of the 150 nm thick coatings deposited by GIMS in the industrial facility (the thickness differences on the large plates with 2000 mm width did not exceed 20 nm) is fully acceptable form the point of view of expected applications e.g. for architectural glazing.

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Characterisation of coloured TiO /Ti/glass systems

Cited by 24 publications

References 27 publications

Optical Properties of Titanium in the Regime of the Limited Light Penetration

Optical Properties of Titanium in the Regime of the Limited Light Penetration

Kesan Pigmen Pewarna terhadap Pertumbuhan Sebatian antara Logam Sambungan Pateri Sn-3.0Ag-0.5Cu

Novel GIMS technique for deposition of colored Ti/TiO₂ coatings on industrial scale

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