1979
DOI: 10.1021/ac50043a071
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Digestion of environmental materials for analysis by inductively coupled plasma-atomic emission spectrometry

Abstract: Aciorojnce-w/UkrArV-Flgure 1. Lead interference at the Sb 217.58-nm line using Sb lamp, 20-µ depositions of 1, 10, 25 pg/tvL Pb and a 0.5-nm (top trace) and a 2-nm bandwidth(2) Spectral Interference by Sb on the Determination of Pb at 217.00 nm. The absorbance of 10 Mg/mL Sb is equivalent to that of 0.005 /¿g/mL Pb, a ratio of about 2000:1. Even this small effect can be avoided by using the very good Pb line at 283.33 nm, where there are no known spectral interferences.(3) Spectral Interference by Ni on the De… Show more

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Cited by 228 publications
(73 citation statements)
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“…A 10 ml sample of urine at each time point was taken and frozen for later analysis of sodium concentration by inductively coupled plasma atomic emission spectrometry (Dahlquist and Knoll, 1978) using a Spectro CIROS ICPAES machine (Waite Analytical Services). Samples were digested with nitric acid and finished with hydrochloric acid as described by McQuaker et al (1979). The intra-assay coefficient of variation for sodium concentration was 2.88%.…”
Section: Experimental Designmentioning
confidence: 99%
“…A 10 ml sample of urine at each time point was taken and frozen for later analysis of sodium concentration by inductively coupled plasma atomic emission spectrometry (Dahlquist and Knoll, 1978) using a Spectro CIROS ICPAES machine (Waite Analytical Services). Samples were digested with nitric acid and finished with hydrochloric acid as described by McQuaker et al (1979). The intra-assay coefficient of variation for sodium concentration was 2.88%.…”
Section: Experimental Designmentioning
confidence: 99%
“…Nitrogen, sodium and other minerals were determined in a commercial laboratory (CSBP Soil and Plant Laboratory, Bibra Lake, WA, Australia) using the standard operating methods for the Thermo Iris Intrepid Duo ICP (X series ICP-MS, Thermo Electron Cooperation, Waltham, MA, USA). Feed was digested by the method of McQuaker et al (1979) prior to the analysis for nitrogen, sodium, chromium and other minerals. Chromium analysis was done in a separate commercial laboratory (CSIRO Analytical Services) using the atomic absorption spectrometer method of Cary and Allaway (1971).…”
Section: Experimental Dietsmentioning
confidence: 99%
“…From the ground samples, subsamples (approximately 5 g) were taken and used in the mineral nutrient analysis. Nitrogen was assayed using the method of Sweeney and Rexroad (1987), minerals such as Ca, Cu, Fe, K, Mg, Mn, Na, P, S, and Zn according to the method of McQuacker et al (1979), chloride and nitrate according to Zall et al (1959), and B following Wolf (1974).…”
Section: Mineral Contentmentioning
confidence: 99%