2013
DOI: 10.1557/jmr.2012.403
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Dislocations with edge components in nanocrystalline bcc Mo

Abstract: We report high-resolution transmission electron microscopy (HRTEM) observation of a high density of dislocations with edge components (;10 16 m À2 ) in nanocrystalline (NC) body-centered cubic (bcc) Mo prepared by high-pressure torsion. We also observed for the first time of the ½,111. and ,001. pure edge dislocations in NC Mo. Crystallographic analysis and image simulations reveal that the best way using HRTEM to study dislocations with edge components in bcc systems is to take images along ,110. zone axis, f… Show more

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Cited by 33 publications
(17 citation statements)
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“…During severe plastic deformation, forest dislocations and a high density of grain boundaries are formed. From recent studies on nanocrystalline bcc-metals with grain sizes smaller 300 nm, it is known that the deformation is mainly governed by edge dislocations [23][24], and the thermally activated contribu-200 tion of screw dislocations is completely omitted for grain 230 230 sizes below 100 nm. This might further affect the time dependent deformation behavior.…”
mentioning
confidence: 99%
“…During severe plastic deformation, forest dislocations and a high density of grain boundaries are formed. From recent studies on nanocrystalline bcc-metals with grain sizes smaller 300 nm, it is known that the deformation is mainly governed by edge dislocations [23][24], and the thermally activated contribu-200 tion of screw dislocations is completely omitted for grain 230 230 sizes below 100 nm. This might further affect the time dependent deformation behavior.…”
mentioning
confidence: 99%
“…[1,2] For example, deformation twinning has been frequently observed even in NC face-centered cubic (fcc) materials that do not deform by twinning in their coarse-grained counterparts. [2,3] Formation of twins in NC metals [2,4,5] plays a critical role in their physical and mechanical properties, such as good electrical conductivity, and excellent resistance to currentinduced diffusion.…”
mentioning
confidence: 99%
“…4b and d. The observed dislocations in NC Mo were mainly from the edge or mixed dislocations [29,42] and their density was almost at the same order of magnitude in both irradiated and unirradiated samples. But most of them in irradiated CG Mo might be from the projection of dislocation loops since no obvious dislocation line was observed via two-beam imaging.…”
Section: O M / L O C a T E / S C R I P T A M A Tmentioning
confidence: 83%
“…Refining the grains of materials into nanometer size can significantly alter the physical, chemical and mechanical behaviors of the materials [25][26][27][28][29][30][31]. Previous reports [32-35] on fcc/bcc nanolayered composites have showed extreme tolerance to He bubbles, which are prone to segregate at interphase boundaries.…”
Section: Introductionmentioning
confidence: 99%