Encyclopedia of Analytical Chemistry 2017
DOI: 10.1002/9780470027318.a2007.pub3
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Dynamic Mechanical Analysis

Abstract: Fundamental aspects of biomineralization may be important in order to understand and improve calcification onto the surface of biomaterials. The biomineralization process is mainly followed in vitro by assessing the evolution of the apatite layer that is formed upon immersion of the material in Simulated Body Fluid (SBF). In this work we propose an innovative methodology to monitor apatite deposition by looking at the evolution of the mechanical/viscoelastic properties of the sample while immersed in SBF, usin… Show more

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Cited by 43 publications
(33 citation statements)
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“…The maximum value of tan δ is called the glass transition temperature ( T g ). The storage modulus of the polymers decreases with temperature while the loss modulus and tan δ rise to the maximum when the temperature approaches the glass transition temperature ( T g ) . In the present work, the storage modulus and tan δ of pure PVA and its composites with CNPs are plotted against temperature ranging from 100 to 150°C.…”
Section: Resultsmentioning
confidence: 99%
“…The maximum value of tan δ is called the glass transition temperature ( T g ). The storage modulus of the polymers decreases with temperature while the loss modulus and tan δ rise to the maximum when the temperature approaches the glass transition temperature ( T g ) . In the present work, the storage modulus and tan δ of pure PVA and its composites with CNPs are plotted against temperature ranging from 100 to 150°C.…”
Section: Resultsmentioning
confidence: 99%
“…These viscoelastic properties of polymers, such as the tire tread compound, are usually determined by means of Dynamic Mechanical Analysis (D.M.A.). This method requires testing a polymeric specimen of suitable dimension within a frequency range from 0.1 Hz to 100 Hz [5]. Furthermore, the D.M.A.…”
Section: Viscoelastic Properties and Characterization Methodsmentioning
confidence: 99%
“…The Dynamic Mechanical Analysis (D.M.A.) is widely employed into the characterization of viscoelasticity in order define the hysteretic behaviour of the compound following the Time-Temperature Superposition principle [5]. On one hand, this testing approach perfectly fits with polymer specimens manufactured with specific dimension for the D.M.A.…”
Section: Introductionmentioning
confidence: 99%
“…DMA measurements can be performed for various loading types. Basics of the DMA are well described in David (1999) and Menard and Menard (2017). In brief, during the measurement a sinusoidal force is applied to the sample, which results to a sinusoidal deformation.…”
Section: Dynamic Mechanical Analysismentioning
confidence: 99%