2018
DOI: 10.3184/174751918x15287934329446
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Efficient Preparation of Potassium Arylmethylene-4-(1H-Pyrazol-5-ol)-4′-(1H-Pyrazol-5-Olate) Derivatives via a Four-Component Reaction

Abstract: A four-component reaction was investigated to prepare potassium arylmethylene-4-(1 H-pyrazol-5-ol)-4′-(1 H-pyrazol-5-olate) derivatives from dialkyl but-2-ynedioates, phenylhydrazine, substituted benzaldehydes and potassium carbonate without any catalyst or promoter. The structure of a typical product was confirmed by X-ray crystallography. The advantages of the present methodology are efficiency, broad scope, operational simplicity, high yields and mild reaction conditions.

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