Fabric phase sorptive extraction: An innovative sample preparation approach applied to the analysis of specific migration from food packaging

Aznar, María Pilar Matud; Alfaro, Pilar; Nerín, Cristina; Kabir, Abuzar; Furton, Kenneth G.

doi:10.1016/j.aca.2016.06.049

Cited by 59 publications

(25 citation statements)

References 29 publications

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“…FPSE ensures high sorption area and selectivity. As any type of extraction solvent can be chosen, the sample can be analyzed not only by GC-MS but also by liquid chromatography [63,64].…”

Section: Volatile Compoundsmentioning

confidence: 99%

Analytical Approaches for Analysis of Safety of Modern Food Packaging: A Review

Wrona

Nerı́n

2020

Molecules

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Nowadays, food packaging is a crucial tool for preserving food quality and has become an inseparable part of our daily life. Strong consumer demand and market trends enforce more advanced and creative forms of food packaging. New packaging development requires safety evaluations that always implicate the application of complex analytical methods. The present work reviews the development and application of new analytical methods for detection of possible food contaminants from the packaging origin on the quality and safety of fresh food. Among food contaminants migrants, set-off migrants from printing inks, polymer degradation products, and aromatic volatile compounds can be found that may compromise the safety and organoleptic properties of food. The list of possible chemical migrants is very wide and includes antioxidants, antimicrobials, intentionally added substances (IAS), non-intentionally added substances (NIAS), monomers, oligomers, and nanoparticles. All this information collected prior to the analysis will influence the type of analyzing samples and molecules (analytes) and therefore the selection of a convenient analytical method. Different analytical strategies will be discussed, including techniques for direct polymer analysis.

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“…FPSE ensures high sorption area and selectivity. As any type of extraction solvent can be chosen, the sample can be analyzed not only by GC-MS but also by liquid chromatography [63,64].…”

Section: Volatile Compoundsmentioning

confidence: 99%

Analytical Approaches for Analysis of Safety of Modern Food Packaging: A Review

Wrona

Nerı́n

2020

Molecules

Self Cite

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“…Afterwards, the extract is centrifuged and filtered before being injected into the analytical instrument. The FPSE process is described schematically in Figure 1 [6,8,9]. The FPSE media can be reused for further extraction procedures by washing with a suitable solvent system and drying on a watch glass so that it can be ready for storage in an air-tight glass container for future use.…”

Section: Introductionmentioning

confidence: 99%

Fabric Phase Sorptive Extraction: Current State of the Art and Future Perspectives

et al. 2018

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Fabric phase sorptive extraction (FPSE) is a novel and green sample preparation technique introduced in 2014. FPSE utilizes a natural or synthetic permeable and flexible fabric substrate chemically coated with a sol-gel organic-inorganic hybrid sorbent in the form of ultra-thin coating, which leads to a fast and sensitive micro-extraction device. The flexible FPSE requires no modification of samples and allows direct extraction of analytes. Sol-gel sorbent-coated FPSE media possesses high chemical, solvent, and thermal stability due to the strong covalent bonding between the substrate and the sol-gel sorbent. Therefore, any elution solvent can be used in a small volume, which achieves a high pre-concentration factor without requiring any solvent evaporation and sample reconstitution step. Taking into consideration the complexity of the samples and the need of further minimization and automation, some new, alternative modes of the FPSE have also been developed. Therefore, FPSE has attracted the interest of the scientific community that deals with sample pre-treatment and has been successfully applied for the extraction and determination of many analytes in environmental samples as well as in food and biological samples. The objective of the current review is to present and classify the applications of FPSE according to different sample categories and to briefly show the progress, advantages, and the main principles of the proposed technique.

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“…Another interesting application of FPSE using UPLC-MS(QqQ) is for migration analysis of several non-volatile additives in food packaging materials [34]. Three different sol-gel coated FPSE media with diverse polarities were investigated: sol-gel PDMS (non-polar), sol-gel PTHF (medium polar) and sol-gel PEG (highly polar) all coated on cellulose substrates as well as several extraction parameters were optimized.…”

Section: Applications Of Fabric Phase Sorptive Extractionmentioning

confidence: 99%

Fabric Sol–gel Phase Sorptive Extraction Technique: A Review

Kazantzi

Anthemidis

2017

Separations

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Since the introduction in 2014 of fabric phase sorptive extraction (FPSE) as a sample preparation technique, it has attracted the attention of many scientists working in the field of separation science. This novel sorbent extraction technique has successfully utilized the benefits of sol-gel derived hybrid sorbents and a plethora of fabric substrates, resulting in a highly efficient, sensitive and green sample pretreatment methodology. The proposed procedure is an easy and efficient pathway to extract target analytes from different matrices providing inherent advantages such as high sample loading capacity and short pretreatment time. The present review mainly focuses on the background and sol-gel chemistry for the preparation of new fabric sorbents as well as on the applications of FPSE for extracting target analytes, from the time that it was first introduced. New modes of FPSE including stir FPSE, stir-bar FPSE, dynamic FPSE, and automated on-line FPSE are also highlighted and commented upon in detail. FPSE has been effectively applied for the determination of various organic and inorganic analytes in different types of environmental and biological samples in high throughput analytical, environmental, and toxicological laboratories.

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Fabric phase sorptive extraction: An innovative sample preparation approach applied to the analysis of specific migration from food packaging

Cited by 59 publications

References 29 publications

Analytical Approaches for Analysis of Safety of Modern Food Packaging: A Review

Analytical Approaches for Analysis of Safety of Modern Food Packaging: A Review

Fabric Phase Sorptive Extraction: Current State of the Art and Future Perspectives

Fabric Sol–gel Phase Sorptive Extraction Technique: A Review

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