Gas Chromatography-Mass Spectrometry (Gc-Ms) Analysis of Consolida Thirkeana Extract

Abstract

Objective: Consolida thirkeana (Boiss.) Bornm. (Ranunculaceae) is considered endemic to Turkey and identified by pale lilac flowers, sessile follicles, and laciniae linear leaves. The genus Consolida can often be confused morphologically with Delphinium, in this respect, members of the genus Consolida need chemotaxonomic interest. In this study, the phytochemical content of C. thirkeana was clarified by GC/MS analysis.Material and Method: The plant material was collected from Ayaş (Ankara/Turkey). A voucher specimen was deposited in the Ankara University Faculty of Pharmacy Herbarium. The aerial part of the plant was powdered in a grinder. The powdered plant parts were macerated with methanol. The GC-MS analysis of extracts was performed using an Agilent 6890 gas chromatograph equipped with an Agilent 5973N quadrupole mass spectrometer (Agilent, USA). Mass Hunter software (Qualitative Analysis B.07.00) and the NIST Mass Spectral Library (2014) were used for determining and identifying compounds.Result and Discussion: The analysis results of this study showed the presence of 15 compounds in C.

Silene Ruscifolia Metanoli̇k Herba Ekstresi̇ndeki̇ Fi̇toki̇myasallarin Lc-Qtof/MS Ve Gc/MS İle İncelenmesi̇

“…The two-step derivatization procedure was performed before the GC/MS analysis. During the procedure, methoxymation followed by silylation was applied before the analysis [28][29].…”