2014
DOI: 10.1155/2014/594873
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Large‐Scale Synthesis of Silver Nanoparticles by Aqueous Reduction for Low‐Temperature Sintering Bonding

Abstract: Silver nanoparticles with average diameter of 22.4 nm were prepared by aqueous reduction method for low-temperature sintering bonding application. The reaction temperature and PVP concentration, which are the influential factors of nanoparticle characteristics, were investigated during reduction process. In our research, monodispersity of nanoparticles was remarkably improved while unfavorable agglomeration was avoided with the AgNO3/PVP mass ratio of 1 : 4 at the reaction temperature 30°C. Besides, copper pad… Show more

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Cited by 18 publications
(7 citation statements)
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“…There are many reports on the potential of AgNP production on a large scale using batch reactors . In general, these investigations focus on the optimum parameters in the synthesis processes such as concentration, time, reducing agent, and stabilizer or combination effects with physical treatment such as heating, stirring, or sintering.…”
Section: Future Challengesmentioning
confidence: 99%
“…There are many reports on the potential of AgNP production on a large scale using batch reactors . In general, these investigations focus on the optimum parameters in the synthesis processes such as concentration, time, reducing agent, and stabilizer or combination effects with physical treatment such as heating, stirring, or sintering.…”
Section: Future Challengesmentioning
confidence: 99%
“…Similarly, several studies have reported the increase of nanoparticle size, with increasing the amount of the stabilizer [29][30][31]. The high concentration of the stabilizer would form a thick polymer layer on the particles, contacting them mutually and exacerbating the agglomeration of nanoparticles [32].…”
Section: Discussionmentioning
confidence: 92%
“…This is in contrast to the other nanoparticles formation methods obtained by other research studies which illustrated the nanoparticles formation of different sizes and interparticle separation as the temperature increased. Also, those methods required subsequent process of annealing temperature as an additional process that showed indirect deposition on the substrate surface [35][36][37][38]. Moreover, the substrate temperature provides sufficient surface mobility to the deposited Ag nanoparticles for diffusion into their growth sites and coalescing to form larger particles [39].…”
Section: Morphological Propertiesmentioning
confidence: 99%