A number of new selective wet etching solutions for AIInP over GaAs and InGaP have been investigated. We find that in addition to HCI and Br2-MeOH, the following room temperature acids also etch AIInP lattice matched to GaAs : HF, HI, H2SO4, HsPO4 and C6H807 (citric acid). Selective etching over GaAs can be obtained with HF, HI, HsPO4 and C6H807, while use of HF, HI, H2SO4, H3PO4, and CeHeO7 provides selectivity over InGaP. The etching of AIInP in HsPO4 is thermally activated, and has the form R o~ exp (-Ea/kT), where Ea = 12.03 kcal 9 moF 1, consistent with the rate-limiting step being chemical reaction at the AIInP surface.