Notizen: Silylierung von Aminosäure-hydrochloriden

Rühlmann, Klaus; Michael, Günter

doi:10.1515/znb-1960-1214

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1962

1976

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Cited by 12 publications

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“…1 L,L-S1-NH-CIlK'-C-~1-~~l3 (11) [43], which are also Formed from the sodium salts [44] or hydrochlorides [45] with trimethylsilyldiethylamine, diethylamine being eliminated. These esters are also formed with particular ease from free amino acids by warming t Iicm in hexamethylsilazane, (H3C)3Si-NHPSi(CH3)~, ammonia being evolved [46].…”

Section: Protecting Groupsmentioning

confidence: 99%

Methods of Peptide Synthesis

Wieland

Determann

1963

Angew. Chem. Int. Ed. Engl.

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Section: Protecting Groupsmentioning

confidence: 99%

Methods of Peptide Synthesis

Wieland

Determann

1963

Angew. Chem. Int. Ed. Engl.

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Peptidsynthesen (V)

Wieland

Determann

1963

Angew. Chem.

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Über die Si‐N‐Bindung, XXIV. Die Umsetsung von Aminosäuren mit Trimethylchlorsilan, II Darstellung un Eigenschaften der Aminosäuresilylester‐hydrochloride

Hills

Rühlmann

1967

Chem. Ber.

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Bei der Umsetzung von freien Aminosauren bzw. Aminosaure-hydrochloriden mit Trimethylchlorsilan oder von N-Trimethylsilyl-aminosaure-trimethylsilylestern rnit der berechneten Menge HCI in Ather entstehen in guten Ausbeuten Aminosaure-trimethylsilylester-hydro- + >Sic1 --R'CO-NH-CHR-COzSi< + HCI (2) und Riihlmann konnte aus Na-Salzen 2) oder Hydrochloridens) von Aminosauren N-Trimethylsilyl-aminosaure-trimethylsilylester darstellen.aminosaure-trimethylsilylester iiber,

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Notizen: Silylierung von Aminosäure-hydrochloriden

Cited by 12 publications

References 0 publications

Methods of Peptide Synthesis

Methods of Peptide Synthesis

Peptidsynthesen (V)

Über die Si‐N‐Bindung, XXIV. Die Umsetsung von Aminosäuren mit Trimethylchlorsilan, II Darstellung un Eigenschaften der Aminosäuresilylester‐hydrochloride

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