Powder agglomeration patterns at acoustic driving observed by sonoluminescence technique

Abstract

A sonoluminescence (SL) technique gives a sensitive probe to detect spatial agglomeration patterns produced in powder mixtures subjected to acoustically driven plate. Studies of the surface-integrated SL intensity with increasing driving amplitude yield data about variations of the packing density on the surface of vibrating powders. Imaging of spatial distributions of the SL intensity enables direct measurement of the size of agglomeration patterns. The size of the patterns is found to be ∼102 μm in a 3-μm-sized powder at a driving frequency of about 4 MHz. The distribution of the average sonoluminescence intensity across the pattern is attributed to the density gradient while rapid variations in the SL intensity across the pattern are suggested to give the particle velocity distribution within the pattern. The temporal changes of the SL intensity can be used to study time evolutions of dense powder arrangements.

Determination of the Degree of Mixing in Multicomponent Ceramic Powder Compacts by Micro‐Raman Spectroscopy

“…However, accurate determination of the mixedness of constituent powders in a powder mixture or a green compact is much more difficult. Techniques such as sonoluminescence 5 and magnetic resonance 6 imaging have been applied to study the defects, voids, and agglomerates in porous ceramics and powder mixtures. The reflection spectra of geological minerals also have been used to estimate the grain size and mixing ratios in fine powder mixtures.…”