Production of nano-bentonite and the study of its effect on mutagenesis in bacteria Salmonella typhimurium

Degtyareva, I.A.; Ezhkova, A.M.; Yapparov, A. Kh.; Yapparov, I. A.; Ежков, В О; Babynin, E. V.; Davletshina, A. Ya.; Motina, T.Yu.; Yapparov, D.A.

doi:10.1134/s1995078016050050

Cited by 7 publications

(6 citation statements)

References 22 publications

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“…For example, He et al (2013) Nano-bentonite is highly efficient in removing Cd and Hg from wastewater with adsorption power of 99.03% and 99.18% (Sirait & Manalu, 2018). Numerous studies demonstrated that n-Be is safe in its nano-size concern mutagenic properties (Degtyareva et al, 2016).…”

Section: Discussionmentioning

confidence: 99%

Remediation of heavy metals in contaminated soil by using nano‐bentonite, nano‐hydroxyapatite, and nano‐composite

El-Nagar

Abdel-Halim

2021

Land Degrad Dev

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Soil and water contaminants have an impact on ecosystems, agricultural productivity, groundwater, and human health. Therefore, it is necessary to develop new technologies to treat pollution, one of these techniques is the use of nanomaterials (NMs).This study aimed to evaluate the efficiency of bentonite nano-sheet structure (n-Be), hydroxyapatite nanoparticles (HapNP), and their nano-composite (n-Be/HapNC) on immobilizing nickel (Ni), copper (Cu), and lead (Pb) in peanut-cultivated soil. The prepared materials were characterized by X-ray powder diffraction, atomic force microscopy, surface area, and Fourier transform infrared. Eight levels of material were used T1 (bentonite, 1 t ha À1 ), T2 (hydroxyapatite, 1 t ha À1 ), T3 (HapNPs, 50 kg ha À1 ), T4 (HapNPs, 100 kg ha À1 ), T5 (n-Be, 50 kg ha À1 ), T6 (n-Be, 100 kg ha À1 ), T7 (n-Be/ HapNC, 50 kg ha À1 ), and T8 (n-Be/HapNC, 100 kg ha À1 ). The results indicated that the available Ni, Cu, and Pb showed a significant decline in the treated soil, in comparison to untreated. Levels of Ni exhibited a decrease in the following order: T8 < T6 < T7 < T5. Similar patterns were observed for Cu and Pb levels, where treatment T8 exhibited the greatest decline compared to the control. Uptake of heavy metals (HM) by peanut components (leaves, stems, and seeds) showed significant declines for the treatments, compared to the control. Treatment (n-Be/HapNC, 100 kg ha À1 ) showed the lowest transfer coefficient of Ni (0.53) and Cu (0.048) compared to control (0.71 and 0.097), respectively. Treatments of NMs significantly exhibited increases in fresh weight, pods, and seeds, compared to the control. From all findings, it is obtained that nano-forms of such materials can immobilize HM in contaminated soil, enhance its characteristics, decrease HM-uptake by plants, and are considered good immobilizers for HM in soil. These materials play a role in treating contaminated soil and thus making it suitable for agriculture.

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Section: Discussionmentioning

confidence: 99%

Remediation of heavy metals in contaminated soil by using nano‐bentonite, nano‐hydroxyapatite, and nano‐composite

El-Nagar

Abdel-Halim

2021

Land Degrad Dev

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“…Почвоведение и агрохимия, №2, 2023 избытке и нарушать экологическое равновесие. Современные технологии биологизации сельского хозяи ства обеспечивают последовательную замену энергоемких минеральных удобрении и пестицидов биопрепаратами нового поколения, разработанными отечественными и зарубежными исследователями [4][5][6]. Таким образом, при применении биоудобрении и биопрепаратов активизируется не только жизнедеятельность растении , но и деятельность микроорганизмов почвы, что способствует повышению урожаи ности культур и улучшению качества продукции.…”

Section: плодородие почвunclassified

“…По результатам наших исследовании , численность азотфиксирующих микроорганизмов во всех исследуемых почвенных образцах была приблизительно одинаковои и составляла 10 6 КОЕ на г почвы, то есть во всех почвенных образцах насчитывались миллионы клеток азотфиксирующих микроорганизмов. Наибольшее количество азотфиксаторов было отмечено в образце почвы с комплексом «Hanse-Plant» ((14,8±0,7)×10 6 ) и последеи ствием биогумуса ((14,2±1,4)×10 6 ), наименьшее -на контроле ((7,5±1,4)×10 6 ). Незначительное повышение по сравнению с контрольным вариантом была на варианте с последеи ствием навоза ((9,2±1,3)×10 6 ) (таблица 5).…”

Section: плодородие почвunclassified

“…На низкии показатель общеи численности почвенных микроорганизмов на пашне, а также при применении навоза было указано в литературных источниках [15][16][17], которая получила подтверждение в наших опытах. И на варианте с последеи ствием навоза, по сравнению с другими биоудобрениями и биопрепаратами, получен относительно низкии показатель численности азотфиксирую-щих микроорганизмов в почвенных образцах ((9,2±1,3)×10 6 ), которое, по-видимому, связано с тем, что разложение навоза приводила к снижению численности аммонифицирующих бактерии участвующих в иммобилизации азота.…”

Section: плодородие почвunclassified

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The influence of biofertilizers and biologics on the fertility and productivity of gray-earth soils of the south-east of Kazakhstan

Kenenbayev,

Yessenbayeva,

Zhanbyrbayev

et al. 2023

ПиА

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The article presents the results of a study on the use of biofertilizers and biologics (biohumus, manure, HansePlant, BioEcoGum, Tumat and Agroflorin) on the indicators of fertility and productivity of gray-earth soils of the south-east of Kazakhstan. In the variants of biofertilizers and biologics, the increase in total humus compared to the control was 0.02-0.04 %. Increase of nitrate nitrogen, respectively (0.4-1.1 mg/kg), mobile elements of phosphorus (10.2-16.3 mg/kg), potassium (14.4-22.2 mg/kg) and sulfur (0.1-0.5 mg/kg). The use of biofertilizers and biological preparations has shown an improvement in the agro- and water-physical properties of the soil. Biofertilizers and biologics contributed to an increase in the quantitative and weight index of large nodules formed on the main root, where active nitrogen fixation occurs (12.2-19.0 pieces or 33.5-49.7 % of all formed nodules). The largest number of nitrogen fixators was also observed in soil samples with biofertilizers and biological preparations (from (9.2±1.3) ×106 to (14.8±0.7)×106). The introduction of biofertilizers and biologics increased the content of protein (34.71-34.92 %) and fat (29.50-30.78 %) in soybean plant samples. According to the content of heavy metals in soybean grain (Zn, Fe, Mn, Ni, Co), the indicators in these variants did not exceed the maximum permissible concentration. On average, in 2021-2022, a higher level (31.4-39.8 c/ha) of soybean grain yield was obtained on variants with biologization means. At the same time, the highest yield was obtained when treated with HansePlant – 39.8 c/ha, slightly lower than 35.2-38.6 c/ha (BioEcoGum and Tumat). On variants with the aftereffect of vermicompost and manure, respectively, 31.4 c/ha were obtained. With the yield under control - 24.2 c/ ha.

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“…Ukuran Nanobentonit pada persebaran 5%, 10%, dan 50% memiliki ukuran partikel sebesar 1,09; 1,83; dan 17,92 μm. Penelitian Degtyareva [13] menghasilkan nanobentonit dengan ukuran antara 25-95 μm, dibandingkan dengan penelitian ini, nanobentonit memiliki persebaran ukuran partikel yang lebih kecil. Pada tahap sonikasi, bentonit mengalami deagregasi, merusak struktur partikel menjadi ukuran yang lebih kecil [14].…”

Section: Efek Berbagai Ph Pada Pengukuran Asam Oksalatunclassified

PENGARUH VARIASI pH TERHADAP PENGUKURAN ASAM OKSALAT DENGAN ELEKTRODA GRAPHENE OXIDE TERMODIFIKASI NANOBENTONIT SECARA SIKLIK VOLTAMETRI THE EFFECT OF VARIOUS pH VALUES ON MEASUREMENT OXALIC ACID USING NANOBENTONITE MODIFIED GRAPHENE OXIDE ELECTRODE BY CY

Setiarso

Saputra

2020

UJC

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Telah dipelajari pengaruh pH pada pengukuran asam oksalat menggunakan elektroda Graphene oxide termodifikasi nanobentonit dengan metode siklik voltametri.Graphene oxide dan nanobentonitmasing-masing telah berhasil disintesis metode Improved Hummer dan Sonochemical. Elektroda dibuat dari campuran Graphene oxide:nanobentonit:parafin dengan perbandingan 3:2:5; 3:3:4; 3:4:3; 3:5:2. Variasi pH yang dipelajari yaitu 3,5; 4; 4,5; 5; dan 5,5. Kedua material tersebut di karakterisasi dengan FTIR dan PSA. Spektrum FTIR Graphene oxide membuktikan bahwa Graphene oxide telah berhasil disintesis dengan memunculkan gugus –OH pada bilangan gelombang3445cm-1., tekukan C=C pada bilangan gelombang1622cm-1, regangan gugus C-O pada bilangan gelombang 1225cm-1 dan regangan gugus epoksi C-O-C pada bilangan gelombang 1042cm-1. Spektrum FTIR nanobentonit menunjukkan serapan kuat pada bilangan gelombang 1028cm-1 menunjukkan regangan gugus Si-O-Si, pada bilangan gelombang 793 cm-1 menunjukkan regangan gugus Al-O-Si. Sementara data PSA menunjukan bahwa distribusi partikel graphene oxide sebanyak 5% berukuran 0,61μm. Data PSA menunjukkan bahwa distribusi partikel nanobentonit sebanyak 5 % berukuran 1.09μm. Hasil penentuan elektroda komposisi terbaik yaitu pada perbandingan komposisi 3:5:2 dengan arus puncak anodik sebesar 3,29x10-3 A. Pengukuran asam oksalat terbaik pada kondisi pH larutan 4,5 dengan arus puncak anodik sebesar 3,76x10-3 A.Kata kunci : voltametri siklik, elektroda Graphene oxide termodifikasi nanobentonit, asam oksalat The effect of pH on the measurement of oxalic acid using nanobentonite modified Graphene oxide electrodes with the cyclic voltammetry method. Graphene oxide and nanobentonite have been successfully synthesized by the Improved Hummer and Sonochemical methods. Electrodes are made from a mixture of Graphene oxide: nanobentonite: paraffin in a ratio of 3:2:5; 3:3:4; 3:4:3; 3:5:2. The pH variations studied were 3.5; 4; 4,5; 5; and 5.5. Both materials were characterized by FTIR and PSA. The FTIR spectrum of Graphene oxide proves that Graphene oxide has been successfully synthesized by raising the -OH group at wave number 3445cm-1. bend C=C at wave number 1622cm-1, the strain of C-O group at wave number 1225cm-1, and strain of epoxy group C-O-C at wave number 1042cm-1. The nanobentonite FTIR spectrum shows strong absorption at wave number 1028cm-1 indicating strain of the Si-O-Si group, at wave number 793 cm-1 indicating the strain of the Al-O-Si group. While the PSA data show that the distribution of graphene oxide particles as much as 5% measuring 0.61μm. PSA data show that the distribution of 5% nanobentonite particles is 1.09μm. The results of the determination of the best composition electrode are at a ratio of 3:5:2 with an anodic peak current of 3.29x10-3 A. The best measurement of oxalic acid at the pH of the solution 4.5 with an anodic peak current of 3.76x10-3 A.Key words: cyvlic voltammetry, nanobentonite modified Graphene oxide electrode, oxalic acid

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Production of nano-bentonite and the study of its effect on mutagenesis in bacteria Salmonella typhimurium

Cited by 7 publications

References 22 publications

Remediation of heavy metals in contaminated soil by using nano‐bentonite, nano‐hydroxyapatite, and nano‐composite

Remediation of heavy metals in contaminated soil by using nano‐bentonite, nano‐hydroxyapatite, and nano‐composite

The influence of biofertilizers and biologics on the fertility and productivity of gray-earth soils of the south-east of Kazakhstan

PENGARUH VARIASI pH TERHADAP PENGUKURAN ASAM OKSALAT DENGAN ELEKTRODA GRAPHENE OXIDE TERMODIFIKASI NANOBENTONIT SECARA SIKLIK VOLTAMETRI THE EFFECT OF VARIOUS pH VALUES ON MEASUREMENT OXALIC ACID USING NANOBENTONITE MODIFIED GRAPHENE OXIDE ELECTRODE BY CY

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