Proceedings of the 5th International Conference on Information Engineering for Mechanics and Materials 2015
DOI: 10.2991/icimm-15.2015.317
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Synthesis of a Polyhedral Oligomeric Silsesquioxane (POSS) containing Phenyl and DOPO (7Ph-T7-DOPO) and its thermal stability

Abstract: Abstract.A new type of polyhedral oligomeric silsesquioxane (POSS) (7Ph-T7-Vinyl) containing phenyl and 9, 10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOPO) was synthesized from phenyltrimethoxysilane, trichlorovinylsilane, and DOPO in high yield. This product was subjected to addition reaction using an AIBN catalyst in toluene. The structure of 7Ph-T7-DOPO was characterized by 1HNMR and FTIR, and 7Ph-T7-DOPO exhibited a crystal structure of (RSiO1.5) n. TGA curve analysis showed the high thermal stabili… Show more

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