Synthesis of bismuth nanoparticles

Wegner, Karsten; Walker, Bernhard; Pratsinis, Sotiris E.

doi:10.1016/s0021-8502(00)90221-0

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2011

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“…If the condensed matter can be obtained as an aerosol, which remains in the gas phase, this highly loaded gas can be injected into the detector. For the production of the aerosols a long-known principle, which has successfully been used [11] and optimized [12] for the synthesis of nano-particles, was adapted and used to construct the CI [13].…”

Section: Introductionmentioning

confidence: 99%

Studying the evaporation behavior of heavy metals by thermo-desorption spectrometry

Ludwig

Lutz

Wochele

et al. 2001

Fresenius J Anal Chem

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"Thermal desorption experiments" were carried out during which heavy metal evaporation was studied by on-line monitoring. This could be achieved by the use of a tubular furnace connected to a heavy metal detector, i.e. an ICP-OES (inductively coupled plasma optical emission spectrometer), by a specially designed and patented interface. The spectrograms typically had a time resolution of four different elements per minute using a conventional (sequentially operating) ICP-OES. This study shows how thermo-desorption spectrometry (TDS) can be applied to study the evaporation of high boiling substances, such as heavy metal and alkali metal compounds. The future scope of the method is discussed.

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Section: Introductionmentioning

confidence: 99%