Technique for static coating of glass capillary columns

Rutten, G.A.F.M.; Rijks, J.A.

doi:10.1002/jhrc.1240010516

Cited by 31 publications

(5 citation statements)

References 4 publications

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“…Actual values of stationary phase densities have been published and for the majority of cases, this approximation is valid. 203 This relationship shows that as the column i.d. decreases, it is necessary to increase the concentration of the coating solution to maintain a constant film thickness.…”

Section: Experimental Aspects Of Column Coatingmentioning

confidence: 95%

Capillary supercritical fluid chromatography

Fjeldsted¹,

Lee²

1984

Anal. Chem.

115

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Section: Experimental Aspects Of Column Coatingmentioning

confidence: 95%

Capillary supercritical fluid chromatography

Fjeldsted¹,

Lee²

1984

Anal. Chem.

115

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“…Before coating the stationary phase, the capillaries were washed and dried by the same method as in previous work [13]. Stationary phases were statically coated by reported methods [15,16] with a slight modification. Both ends of the capillary column were connected to PTFE tubing (0.5 mm i.d.…”

Section: Column Preparationmentioning

confidence: 99%

Use of crosslinked polysiloxane stationary phases in open‐tubular capillary liquid chromatography

Takeuchi

Kitamura

Spitzer

et al. 1983

J. High Resol. Chromatogr.

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“…The etched columns were coated by the static method as described by Rutten and Rijks [7]. The amount of stationary phase used was adjusted so that the partition ratio (k') of the compounds used for evaluating the phase was greater than 2.5.…”

Section: Column Preparationmentioning

confidence: 99%

Derivatives of cholesterol cinnamate: A comparison of the separations of geometrical isomers when used as gas chromatographic stationary phases

Heath

Doolittle

1983

J. High Resol. Chromatogr.

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Summaryfour para-substituted cholesterol cinnamates were synthesized and evaluated for utility as gas chromatograph (GC) liquid crystal stationary phases. The capability of the phases to separate olefinic geometrical isomers was found to be dependent on the position of the olefinic bond. When unsaturation occurred at positions four carbons or greater from the terminal methyl of the compounds investigated, the relative ability of the phases to separate geometrical isomers was p-CIWhen unsaturation occurred at positions four carbons or less from the terminal methyl the relative ability of the para-derivatives of cholesterol cinnamate to separate geometrical isomers was reversed.

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Technique for static coating of glass capillary columns

Cited by 31 publications

References 4 publications

Capillary supercritical fluid chromatography

Capillary supercritical fluid chromatography

Use of crosslinked polysiloxane stationary phases in open‐tubular capillary liquid chromatography

Derivatives of cholesterol cinnamate: A comparison of the separations of geometrical isomers when used as gas chromatographic stationary phases

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