Total polyphenols quantification in Acridocarpus orientalis and Moringa peregrina by using NIR spectroscopy coupled with PLS regression

Ali, Liaqat; Mabood, Fazal; Rizvi, Tania Shamim; Rehman, Najeeb Ur; Arman, Muhammad; Al-Shidani, Sulaiman; Al-Abri, Zahra; Hussain, Javid; Al‐Harrasi, Ahmed

doi:10.1016/j.cdc.2018.01.005

Cited by 9 publications

(9 citation statements)

References 22 publications

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“…the ATR‐NIR and ATR‐NIR absorbance) and variable matrix y (i.e. the real content of TP) . PLS follows a two‐step strategy to establish a functional relationship between X and y .…”

Section: Methodsmentioning

confidence: 99%

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Assessment of ATR‐NIR and ATR‐MIR spectroscopy as an analytical tool for the quantification of the total polyphenols in Dendrobium huoshanense

Hao

Chen

2020

Phytochemical Analysis

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In this study, the potentiality of applying attenuated total reflectance near‐infrared (ATR‐NIR) and attenuated total reflectance mid‐infrared (ATR‐MIR) techniques combined with a partial least squares (PLS) regression technology to quantify the total polyphenols (TPs) in Dendrobium huoshanense (DHS) was investigated and compared. The real TP contents in the DHS samples were analysed using methods of reference. The capability of the two IR spectroscopic techniques to quantify the TPs in DHS was assessed by the root‐mean‐square error of calibration (RMSEC) and determination coefficients (R2). The results showed that both NIR and MIR might be used as a fast and simple tool to replace traditional chemical assays for the determination of the TP contents in DHS, and the best NIR model showed slightly better prediction performance [root‐mean‐square error of prediction (RMSEP): 0.307, R2: 0.9122, ratio performance deviation (RPD): 4.43] than the best MIR model (RMSEP: 0.440, R2: 0.9069, RPD: 3.09). Results from this study indicated that both the NIR and MIR models could be used to quantify the TP in DHS, and ATR‐NIR appeared to be the more predominant and more robust technique for the quantification of the TP in DHS.

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“…the ATR‐NIR and ATR‐NIR absorbance) and variable matrix y (i.e. the real content of TP) . PLS follows a two‐step strategy to establish a functional relationship between X and y .…”

Section: Methodsmentioning

confidence: 99%

“…the real content of TP). 16 PLS follows a two-step strategy to establish a functional relationship between X and y. First, the input variable matrix X (n, m) and output variable matrix y (n, 1) were decomposed as follows:…”

Section: Pls Regression Is One Of the Most Common Regression Algorithmsmentioning

confidence: 99%

Assessment of ATR‐NIR and ATR‐MIR spectroscopy as an analytical tool for the quantification of the total polyphenols in Dendrobium huoshanense

Hao

Chen

2020

Phytochemical Analysis

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“…Polyphenolic compounds are widely known today as antioxidant, antimicrobial, antiviral and anti-inflammatory agents, becoming desirable plant metabolites and being frequently used in the treatment of specific pathological conditions [ 15 , 16 , 17 , 18 ].…”

Section: Introductionmentioning

confidence: 99%

“…Different analytical methods such as high performance liquid chromatography (HPLC), gas chromatography (GC) or combinations of these analyses with mass spectrometry (MS) are currently employed in the determination of phenolic compounds [ 3 , 19 , 20 , 21 , 22 ]. Even though efficient, for they provide rapid separation and quantification of phenolic compounds, these techniques also require a lot of pre-processing steps before and during the analysis [ 17 , 22 ].…”

Section: Introductionmentioning

confidence: 99%

“…Recently, NIR spectroscopy (coupled with multivariate analyses) has also found excellent potential for quick and inexpensive quantification of total polyphenolic content (TPC) [ 29 ]. The technique has been recently applied (either at-line or on-line ) to determine the content of phenolic compounds in yerba mate [ 22 ], the total content of emodin, chrysophanol, rhein, aloeemodin, and physcion in Rhei Radix et Rhizoma [ 30 ], for the simultaneous testing of total polyphenols, caffeine and free amino acids in Chinese tea from different categories [ 31 ], for measuring the phenolic composition of propolis [ 32 ], as well as for the total polyphenols quantification in Acridocarpus orientalis and Moringa peregrina [ 17 ].…”

Section: Introductionmentioning

confidence: 99%

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Development of a NIR Method for the In-Line Quantification of the Total Polyphenolic Content: A Study Applied on Ajuga genevensis L. Dry Extract Obtained in a Fluid Bed Process

et al. 2018

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This study describes an innovative in-line near-infrared (NIR) process monitoring method for the quantification of the total polyphenolic content (TPC) of Ajuga genevensis dry extracts. The dry extract was obtained in a fluidized bed processor, by spraying and adsorbing a liquid extract onto an inert powder support. NIR spectra were recorded continuously during the extract’s spraying process. For the calibration of the in-line TPC quantification method, samples were collected during the entire process. The TPC of each sample was assessed spectroscopically, by applying a UV-Vis reference method. The obtained values were further used in order to develop a quality OPLS prediction model by correlating them with the corresponding NIR spectra. The final dry extract registered good flowability and compressibility properties, a concentration in active principles three times higher than the one of the liquid extract and an overall process yield of 85%. The average TPC’s recovery of the NIR in-line prediction method, compared with the reference UV-Vis one, was 98.7%, indicating a reliable monitoring method which provided accurate predictions of the TPC during the process, permitting a good process overview and enabling us to establish the process’s end point at the exact moment when the product reaches the desired TPC concentration.

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Secondary metabolites from acridocarpus orientalis inhibits 4T1 cells and promotes mesenchymal stem cells (MSCs) proliferation

et al. 2020

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Total polyphenols quantification in Acridocarpus orientalis and Moringa peregrina by using NIR spectroscopy coupled with PLS regression

Cited by 9 publications

References 22 publications

Assessment of ATR‐NIR and ATR‐MIR spectroscopy as an analytical tool for the quantification of the total polyphenols in Dendrobium huoshanense

Assessment of ATR‐NIR and ATR‐MIR spectroscopy as an analytical tool for the quantification of the total polyphenols in Dendrobium huoshanense

Development of a NIR Method for the In-Line Quantification of the Total Polyphenolic Content: A Study Applied on Ajuga genevensis L. Dry Extract Obtained in a Fluid Bed Process

Secondary metabolites from acridocarpus orientalis inhibits 4T1 cells and promotes mesenchymal stem cells (MSCs) proliferation

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