To obtain complex shape alumina ceramic parts, a composite powder of epoxy resin binder E-06 and alumina powder are laser sintered combined with cold isostatic pressing(CIP). An orthogonal experiment is carried out to probe the influencing factors of selective laser sintering (SLS) alumina green parts. When preheating temperature, laser power, scan speed, scan spacing and layer thickness are, respectively, 60°C,14 w, 2000 mm/s, 0.10 mm/s and 0.10 mm, the density and bending strength of alumina parts are relatively high. Then, airproof canning prepared for CIP is manufactured in the vacuum environment. Finally, the optimized SLS/CIP alumina parts are degreased and sintered in 1600 °C to produce crack-free alumina parts. The sintered relative density of the parts however is limited to only 57% but the forming integrity during SLS and CIP remains after sintering.
Transparent conducting aluminum-doped zinc oxide (AZO) films have been prepared on soda-lime glass substrates by radio frequency magnetron sputtering using a high density ceramic target at different substrate temperatures. The structural, morphology, electrical, and optical properties of the AZO thin films were investigated by X-ray diffraction, scanning electron microscope, Hall measurement, and optical transmission spectroscopy, and which were strongly influenced by substrate temperatures. Films with better texture, higher transmission, lower resistivity and larger carrier concentration were obtained for the samples fabricated at higher substrate temperature. The AZO film with the lowest resistivity of 4.63×10−4 Ω.cm and an average optical transmission of 92% in the visible range was deposited on the substrate heated at 450 °C. The optical bandgap depends on the deposition condition, and was in the range of 3.35~3.59 eV.
A coating methods and the structure of Low-E glass are described in this paper, and the optical and thermal properties of the samples are analyzed as well. The results show that the Low-E glass has a high transmittance in visible region and with a higher reflectance in middle-infrared band and far-infrared band. It can effectively prevent the heat through the glass. Therefore, Low-E glass can save energy by letting enough sunlight into the room and by impeding the heat through the glass effectively.
Al2O3 ceramics with CaO-SiO2-MgO (CMS), Yb2O3 and ZrO2 additives were fabricated by a conventional solid-state reaction method. The effects of ZrO2 dopant on phase compositions, microwave dielectric properties and dielectric breakdown strength of Al2O3 ceramics were studied. XRD demonstrated that CaAl2Si2O8 and Zr &Y compound phases co-existed with alumina. SEM exhibited that ZrO2 dopant could refine the grain of alumina ceramics and improve its relative density. With ZrO2 content increasing from 1wt% to 5wt% εr increased from 9.8 to 10.25, but Q×f decreased from 52823GHz to 35922GHz. The breakdown strength increased initially and reached the maximum value at ZrO2=3wt%. When ZrO2 content is 3wt%, the comprehensive performances were the best: Eb= 37.37kV/mm for 1mm samples and 17.26kV/mm for 3mm samples, Q×f = 37044 GHz, εr = 10.01, and τf = -52 ppm/°C.
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