In order to realize a micro-mechanic performance test of biaxial tensile-bending-combined loading and solve the problem of incompatibility of test apparatus and observation apparatus, novel biaxial-combined tensile-bending micro-mechanical performance test apparatus was designed. The working principle and major functions of key constituent parts of test apparatus, including the servo drive unit, clamping unit and test system, were introduced. Based on the finite element method, biaxial tensile and tension-bending-combined mechanical performances of the test-piece were studied as guidance to learn the distribution of elastic deformation and plastic deformation of all sites of the test-piece and to better plan test regions. Finally, this test apparatus was used to conduct a biaxial tensile test under different pre-bending loading and a tensile test at different rates; the image of the fracture of the test-piece was acquired by a scanning electron microscope and analyzed. It was indicated that as the pre-bending force rises, the elastic deformation phase would gradually shorten and the slope of the elastic deformation phase curve would slightly rise so that a yield limit would appear ahead of time. Bending speed could exert a positive and beneficial influence on tensile strength but weaken fracture elongation. If bending speed is appropriately raised, more ideal anti-tensile strength could be obtained, but fracture elongation would decline.
To enhance the wear resistance of high chromium cast iron (HCCI, Cr26), a new wear resistant alloy with high vanadium and chromium contents (HCCI-V, 15Cr5V4MoSiMn) was designed and prepared by sand mold casting. The microstructure and the phase composition were analyzed by SEM, EDS and XRD, and the abrasive wear property was tested compared with HCCI. Results show that the new wear resistant alloy is characterized by multi-scale and multi-type carbides distributed in a metal matrix composed of martensite and retained austensite. The carbides include VC, M7C3, M2C and M23C6 (M stands for (Cr, Fe)), with dimensions ranging from tens of nanometers to tens of micrometers. The hardness and impact toughness of HCCI-V are 65 ± 0.2 HRC and 10 ± 0.12 J cm−2, respectively, far higher than that of HCCI (57 ± 0.2 HRC, 8 ± 0.12 J cm−2). When the abrasive particle size and load are 6.5 μm and 1.41 MPa respectively, the wear weight loss of HCCI and HCCI-V are 5.6 ± 0.1 mg and 0.8 ± 0.1 mg respectively, and the relative wear resistance of HCCI-V is 7. The excellent wear resistance of HCCI-V is attributed to the multi-scale carbides. The micro-scale carbides resist scratch, and the nano-scale carbides strengthens matrix. The multi-scale carbides can work collaboratively to resist abrasive wear efficiently.
The microstructure and mechanical properties of pure W, sintered and swaged W-1.5ZrO2 composites after 1.5 × 1015 Au+/cm2 radiation at room temperature were characterized to investigate the impact of the ZrO2 phase on the irradiation resistance mechanism of tungsten materials. It can be concluded that the ZrO2 phase near the surface consists of two irradiation damage layers, including an amorphous layer and polycrystallization regions after radiation. With the addition of the ZrO2 phase, the total density and average size of dislocation loops, obviously, decrease, attributed to the reason that many more glissile 1/2<111> loops migrate to annihilate preferentially at precipitate interfaces with a higher sink strength of 7.8 × 1014 m−2. The swaged W-1.5ZrO2 alloys have a high enough density of precipitate interfaces and grain boundaries to absorb large numbers of irradiated dislocations. This leads to the smallest irradiation hardening change in hardness of 4.52 Gpa, which is far superior to pure W materials. This work has a collection of experiments and conclusions that are of crucial importance to the materials and nuclear communities.
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