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ChemInform Abstract (Ag(IO6)2)7-, are studied in basic solution using Pt microelectrodes. From voltammetric and chronoamperometric results it is concluded that the electrochemical reduction of the periodate complex occurs via two electrochemical steps ((Ag(IO6)2)7-→ (Ag(OH)2)-→ Ag) with the final product deposited on the electrode surface. The Ag(III) periodate complex may decompose in aqueous solution yielding the aquo species (Ag(OH)2(IO6)(H2O))4-.