In this paper, the microstructure of Cu82.3Al8.3Mn9.4 (in wt. %) shape memory alloy after hot and cold rolling was investigated. The Cu82.3Al8.3Mn9.4 alloy was produced by a vertical continuous casting method in the form a cylinder rod of 8 mm in diameter. After the casting, hot and cold rolling was performed. By hot rolling a strip with a thickness of 1.75 mm was obtained, while by cold rolling a strip with a thickness of 1.02 mm was produced. After the rolling process, heat treatment was performed.Heat treatment was carried out by solution annealing at 900 °C held for 30 minutes and water quenched immediately after heating. The microstructure characterization of the investigated alloy was carried out by optical microscopy (OM), scanning electron microscopy (SEM) equipped with a device for energy dispersive spectroscopy (EDS). Phase transformation temperatures and fusion enthalpies were determined by differential scanning calorimetry (DSC) method. The homogenous martensite microstructure was confirmed by OM and SEM micrographs after casting. During rolling the two-phase microstructure occurred. Results of DSC analysis showed martensite start (Ms), martensite finish (M f ), austenite start (A s ) and austenite finish (A f ) temperatures.
The Au-Ge alloy is useful for bonding applications in microelectronic and optoelectronic packages. Also, recent investigations show that Au-Ge system could present a lead-free solder candidate. The results of characterization of the eutectic alloy from binary Au-Ge system are presented in this paper. Experimental research was done using thermal analysis (differential thermal analysis, DTA) and structural investigation by light optic microscopy (LOM) and scanning electron microscopy with EDS (SEM-EDS). The eutectic temperature of 359 °C was detected using thermal analysis, while eutectic structure was confirmed using microstructural analysis. Obtained results were compared with recent literature references and good mutual agreement was noticed.
Precipitation hardening stainless steel 17-7PH with modified chemical composition was heat treated by modified RH950 condition. In this paper is presented the results of tests of microstructure and mechanical properties of precipitation hardened stainless steel 17-7PH with modified chemical composition, heat treated in modificated RH950 conditions. Regression analysis showed which variables are statistically significant in predicting the value of mechanical properties of the steel 17-7PH chemically modified composition.
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