In this work, boro-telluride glasses with additional zinc, aluminum, and alkali-alkaline modifiers have been synthesized using the melt-quenching-annealing method. Six glasses were fabricated with composition of [(60 − x)B₂O₃-(10 + x)TeO₂-10ZnO-10Al₂O₃ 5Li₂O-5MgO] all in mol% and x varied from 0, 10, 20, 30, 40 and 50. The aim of this work is to understand the effect of changing the main glass former from B₂O₃ → TeO₂, to obtain new optical materials. To confirm the amorphous nature of these six glasses, X-ray diffraction was characterized for all six glasses from 10° to 80°. Optical absorption with wavelength range 200-800 nm in room temperature was measured, and the optical absorption coefficient α(λ) calculated to obtain the cutoff wavelength. In addition, gamma photons shielding features of the prepared K1-K6 glasses were evaluated by means of some essential parameters such as mass attenuation coefficients (μ/ρ) and effective atomic number (Zeff) at five energies between 0.356 and 1.33 MeV. No significant difference between the theoretical and simulation μ/ρ values was found. The effective atomic number results indiacte that as the TeO₂ content increases, the photons' attenuation increases. The number of interactions of gamma photons with K6 sample (which contains the maximum amount of TeO₂) is relatively high (in comparison to the rest of the samples), which results in more attenuation and thus better shielding features for K6.
This paper deals with electrical characterization of PiN diodes fabricated on an 8° off-axis 4H-SiC with a p++localized epitaxial area grown by Vapour-Liquid-Solid (VLS) transport. It provides for the first time evidence that a high quality p-n junction can be achieved by using this technique followed by a High Temperature Annealing (HTA) process.
The formation of low resistivity ohmic contacts to p-type 4H-SiC is achieved. Transfer Length Method (TLM) based-structures were fabricated on 0.8 µm-thick epitaxial ptype Silicon Carbide (4H-SiC) layers. TLM metal patterns were obtained by a lift-off procedure and electron beam deposition of Ni, Ti and Al. The electrical properties of the contacts were examined using current/voltage measurements. Contact resistivity as a function of annealing was investigated over the temperature range from 700°C to 1000°C. The lowest contact resistivity of 1.5×10 -5 Ω.cm 2 was obtained for Ni/Ti/Al/Ni contact after annealing at 800°C for 90s. Using Secondary Ion Mass Spectrometry (SIMS), Energy-Dispersive X-Ray spectroscopy (EDX) and X-Ray Diffraction (XRD) measurements we quantitatively and qualitatively determined the formation and the nature of the ohmic contact to p-type SiC.
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