Low-temperature electronics operating in below zero temperatures or even below the lower limit of the common −65 to 125 °C temperature range are essential in medical diagnostics, in space exploration and aviation, in processing and storage of food and mainly in scientific research, like superconducting materials engineering and their applications—superconducting magnets, superconducting energy storage, and magnetic levitation systems. Such electronic devices demand special approach to the materials used in passive elements and sensors. The main goal of this work was the implementation of a fully transparent, flexible cryogenic temperature sensor with graphene structures as sensing element. Electrodes were made of transparent ITO (Indium Tin Oxide) or ITO/Ag/ITO conductive layers by laser ablation and finally encapsulated in a polymer coating. A helium closed-cycle cryostat has been used in measurements of the electrical properties of these graphene-based temperature sensors under cryogenic conditions. The sensors were repeatedly cooled from room temperature to cryogenic temperature. Graphene structures were characterized using Raman spectroscopy. The observation of the resistance changes as a function of temperature indicates the potential use of graphene layers in the construction of temperature sensors. The temperature characteristics of the analyzed graphene sensors exhibit no clear anomalies or strong non-linearity in the entire studied temperature range (as compared to the typical carbon sensor).
Microjoining technologies are crucial for producing reliable electrical connections in modern microelectronic and optoelectronic devices, as well as for the assembly of electronic circuits, sensors, and batteries. However, the production of miniature sensors presents particular difficulties, due to their non-standard designs, unique functionality and applications in various environments. One of the main challenges relates to the fact that common methods such as reflow soldering or wave soldering cannot be applied to making joints to the materials used for the sensing layers (oxides, polymers, graphene, metallic layers) or to the thin metallic layers that act as contact pads. This problem applies especially to sensors designed to work at cryogenic temperatures. In this paper, we demonstrate a new method for the dynamic soldering of outer leads in the form of metallic strips made from thin metallic layers on ceramic substrates. These leads can be used as contact pads in sensors working in a wide temperature range. The joints produced using our method show excellent electrical, thermal, and mechanical properties in the temperature range of 15–300 K.
The article presents the results of dynamic tests of the most popular temperature sensors at low temperatures. The resistance sensors (Pt100) and thermocouples (type E and T) were tested. Measurements were carried out in the vacuum cryostat cooled by the closed cycle helium crycooler. The analysis of the temperature characteristics of sensors, the sensitivity and the influence of external factors on the measurement were presented in the paper. Streszczenie. W artykule przedstawiono wyniki badań dynamicznych najbardziej popularnych czujników temperatury w warunkach kriogenicznych. Badaniom zostały poddane czujniki rezystancyjne (Pt100) oraz czujniki termoelektryczne (typ E i T). Pomiary zostały zrealizowane w kriostacie próżniowym współpracującym z kriochłodziarką helową. Przedstawiono analizę charakterystyk temperaturowych czujników, ich czułości oraz wpływ czynników zewnętrznych na pomiar. Właściwości dynamiczne czujników temperatury w warunkach kriogenicznych.
Purpose Passive conducting elements are the important parts of textronic systems. This paper aims to study a possibility of creating well-conducting and durable elements in textile materials by combining two technologies – physical vapour deposition (PVD) and laser patterning. Design/methodology/approach Thin conducting metallic layers on common fabrics do not provide satisfactory resistance to bending and stretching; therefore, selected textile composite materials have been proposed as a substrate. The conducting elements were produced in two stage process – deposition of thin metallic layer on textile composite and creating conducting elements by laser patterning. Laser ablation process was optimized using modelling in Comsol Multiphysics package. Properties of conducting structures were investigated experimentally and by modelling. Findings This paper confirms the correctness of the choice of the textile composite as a substrate for conducting elements. The results have shown that combining PVD deposition of thin metallic layer and controlled laser ablation allow creating passive elements such as resistors, inductive coils and heaters. Computer simulations conducted in the Comsol Multihysics environment enabled to determine the temperature distribution around the heaters and to describe the dynamics of its changes. The obtained results allow to shorten time of the optimization process of structures with different geometry and assumed temperature distribution. Originality/value The novelty of this research can be summarized as following: choosing of textile composites as substrates for conductive elements instead of textiles used so far in textronics; creating conductive structures on textile composites using combined technologies, PVD and laser patterning, for the first time; modelling of laser ablation process of thin metallic layer; and optimization of properties of conducting elements by computer modelling.
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