The particle diameter and luminous intensity of aluminum powder were measured by laser analyzer and photo-effect tester. The luminous intensity of [Ba(NO3)2+Al] illuminant were studied for different shape and diameter of aluminum powder as well as ultra-fine powder prepared by chemical method. The results show that the luminous intensity increases with particle size reduced, and luminous intensity of non-spherical aluminum is more than that of spherical aluminum. The change rate of luminous intensity increases rapidly when particle diameter was less than 2μm. It’s change rate in [0.6,2.13] is 4.37 times that in [2.13,4.24] interval.The ultra-fine aluminum powder and the submicron aluminum powder can effectively enhance the luminous performance of pyrotechnics.
A strong basal plane texture of AZ31 magnesium alloy was obtained by severe hot-rolling with three passes falling temperature. The effects of annealing time and annealing temperature on the evolution of texture at different layers were studied by means of X-ray texture analysis. The results showed that the orientation density of basal plane texture component was reduced greatly tending to dispersion with increasing annealing time and temperature. The hard orientation can be greatly weakened by softening annealing, the best basal plane orientation was obtained when the annealing time is 60min and the annealing temperature is 150~300°C. A texture gradient along thickness direction with annealing has been found in the sheet. The texture gradient was the lowest when the annealing time is 60min and the annealing temperature is 300°C.
NiCoCrAlYSiHf coatings have been prepared by arc ion plating (AIP) on CrNi3MoVA steel ,which their microstructure and isothermal oxidation behavior at 950°C studied using SRD,SEM and EDAX. The results indicate that NiCoCrAlYSiHf coatings substantially increase the high-temperature oxidation resistance of CrNi3MoVA steel and the oxidation process was retarded mainly by the presence of α-Al2O3 oxide scale on the coating. Meanwhile, the major diffusion occured between the substrate element Fe and the coating element Co while Cr mainly distributed in the coating.
ZrO2-MgO and Mo powder coating on a substrate material prepared by an high temperature plasma spraying forming (PSF) for lease-shaped engine nozzles, and its total thickness is about 300 μ m. The surface coating changes of microstructure were investigated by a small solid rocket motor static ablation and the results were discussed for preliminary ions after ablation. The results show that the plasma spraying throat coat is a layer structure and the pore consist in micro-gap between layer and layer.That throat coating erosion is so severe were found after the ablation test , which is because of the metal oxide particles caused by mechanical denudation and high temperature thermal chemical ablation.Whereas the coating interface have no significant cracks after erosion, so that the composite coating of ZrO2-MgO and Mo wear good erosion performance.
The removal effect of nitrobenzene (NB) in water by VUV/O3/GAC synergetic catalyzing method in a nebulizing system was studied. In addition, the effects of the droplet size, the nebulization height, O3 flux, free radical scavengers and active carbon usage frequencies on the degradation of NB were investigated. In this study, a spray nozzle that could produce 10-micrometer droplets were adopted, a UV lamp that emitted 185nm VUV light was used as the light source and a layer of 0.5cm granular active carbon was laid at the bottom of the experimental apparatus. The results showed that, in the apparatus, when the NB concentration in deionized water was 200mg/L, the nebulization height was 1.3m, O3 flux was 150mg/L, the removal rate of NB reached 95.3%. Supercarbonate acted as a catalyst in the system.
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