The electron beam additive manufacturing (EBAM) method was applied in order to fabricate rectangular-shaped NiTi component. The process was performed using an electron beam welding system using wire feeder inside the vacuum chamber. NiTi wire containing 50.97 at.% Ni and showing martensitic transformation near room temperature was used. It allowed to obtain a good quality material consisting of columnar grains elongated into the built direction growing directly from the NiTi substrate, which is related to the epitaxial grain growth mechanism. As manufactured material showed martensitic and reverse transformations diffused over the temperature range from −10 to 44 °C, the applied aging at 500° C moved the transformation to higher temperatures and transformation peaks became sharper. The highest recoverable strain of about 3.5% was obtained in the as-deposited sample deformed along the deposition direction. In the case of deformation of the alloy aged at 500 °C for 2h, the formation of martensite occurs at significantly lower stress; however, at about 2.5% the stress begins to increase gradually and only a small shape recovery was observed due to a higher martensitic transformation temperature. In situ SEM tensile deformation in the direction perpendicular to deposition direction showed that the martensite began to appear at the surface of the sample and at the grain boundaries due to heterogeneous nucleation. In situ studies allowed to determine the following crystallographic relationships between B2 and B19’ martensite: (100)B2||(100)B19’ and (100) B2 || (011)B19’; (011)B2|| (001)B19’ and $${(011)}_{\mathrm{B}2}||{\left(11\bar{1 }\right)}_{\mathrm{B}1{9}^{\mathrm{^{\prime}}}}$$ ( 011 ) B 2 | | 11 1 ¯ B 1 9 ′ . Samples aged at 500 °C exhibited fully austenitic microstructure; however, with increasing degree of deformation, the formation of martensite was observed. The majority of needles were tilted about 45° with respect to the tensile direction, and the presence of type I (11 $$\bar{1 }$$ 1 ¯ ) invariant twin boundaries was observed at higher degrees of deformation.
Nickel-based alloys are widely used in industries such as the aircraft industry, chemicals, power generation, and others. Their stable mechanical properties in combination with high resistance to aggressive environments at high temperatures make these materials suitable for the production of components of devices and machines intended for operation in extremely difficult conditions, e.g. in aircraft engines. This paper presents the results of thermal and mechanical tests performed on precision castings made of the Inconel 713C alloy and intended for use in the production of low pressure turbine blades. The tests enabled the determination of the nil strength temperature (NST), the nil ductility temperature (NDT), and the ductility recovery temperature (DRT) of the material tested. Based on the values obtained, the high temperature brittleness range (HTBR) and the hot cracking resistance index were determined. Metallographic examinations were conducted in order to describe the cracking mechanisms. It was found that the main cracking mechanism was the partial melting of grains and subsequently the rupture of a thin liquid film along crystal boundaries as a result of deformation during crystallisation. Another cracking mechanism identified was the DDC (Ductility Dip Cracking) mechanism. The results obtained provide a basis for improving precision casting processes for aircraft components and constitute guidelines for designers, engineers, and casting technologists.
In the present study, the characteristics of Nd:YAG laser welded joints of 600 MPa DP steel (HDT580X), 2.4 mm in thickness, in respect of hardness, microstructures and mechanical properties were investigated. The test joints have been welded under a shielding gas on the stand for robotic Nd:YAG laser welding at the beam power of 1.5 kW and 2.0 kW. Three combinations of welding parameters were used: 2.0 kW - 2.1 m/min, 2.0 kW - 1.5 m/min and 1.5 kW - 1.2 m/min. Detailed examinations were performed on the joint welded at the highest speed. The microstructure was examined by the optical-, scanning- and transmission electron microscope. The heat affected zone (HAZ) was composed of ferrite, bainite and lath martensite, the weld contained lath martensite. The maximum hardness in the HAZ did not exceed 343 HV. The tensile strength of the welded joint was at the same level as that of the base material. The results of fatigue tests and residual stress measurement of laser welded DP steel joints are also presented. The fatigue strength of the welded joint is lower than that of the base material. The fatigue class FAT was determined, which is equal to 284 MPa - for the base material and 150 MPa – for the welded joint. By means of the modified hole drilling method the following residual stresses were measured: σmax = 573 MPa and σmin= -126 MPa.
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