Air-assisted liquid–liquid microextraction (AALLME) is a procedure for sample preparation that has high recoveries and high preconcentration factors while using a small amount of extractants. This procedure has gained widespread acceptance among scientists due to a variety of advantages, including its easiness, being cheap, green, and available in most laboratories. The current review has focused on the analysis of medicines and organic compounds using various modes of AALLME. The use of various extractants and support factors were developed in many modes of AALLME. A review of literature revealed that the procedure is used as a powerful and efficient approach for extracting medicals and organic compounds. This review explained 12 different types of AALLME methods. The findings on the modifications of AALLME modes that have been published are summarized. Future directions are also being discussed.

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